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GCMS reference analysis results for sample AE06337, May 3 2002

Machine-extracted title · confidence 100%

Reference analysis report for GCMS testing of volatile organic compounds with quantified concentrations recorded on May 3 2002.

NYC-WTC_000044478–000044495

Folder label: “GCMS X 4/29/02 A 5/1/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\050102\6337.D Vial: 13 Acq On 1 May 2002 7:29 pm Operator: Mclean Sample re-ext 4/29 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 02 12:08:24 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Thu May 02 12:07:14 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.94 152 4779324 40.00 ug/L 0.01 10) Napthalene-d8 13.44 136 19095993 40.00 ug/L 0.00 17) Acenapthalene-dlO 18.57 164 10202702 40.00 ug/L 0.00 29) Phenanthranene-dlO 22.96 188 15059239 40.00 ug/L 0.00 37) Chrysene-dl2 30.81 240 11967661 40.00 ug/L 0.00 43) Perylene-dl2 34.72 264 8469178 40.00 ug/L 0.00

System Monitoring Compounds 2 7) TCMX 20.54 207 542283 6.74 u< 0.00 Spiked Amount 10.000 Recovery = 67.40% 50) 2,4-ddd 0.00 235 0 0.00 ug/L Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 41) Bis(2-ethylhexyl)phthalate 31.39 149 503953 1.70 ug/L 96

(#) = qualifier out of range (m) = manual integration (+) = signals summed 6337.D 050102.M Thu May 02 12:18:43 2002 Page 1

NYC-WTC_000044480

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NYC-WTC_000044480Source: NYC Law Department, mirrored locally

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