GCMS reference analysis results for sample AE06338, May 2 2002

2 2 K Quantitation Report (QT Reviewed) K o O

2 Data File C:\MSDCHEM\1\DATA\050102\0429REFB.D Vial: 12 co — o Acq On 1 May 2002 6:40 pm Operator: Mclean "O I C o Sample Inst : Instrumen O o o o Mise : Multiplr: 1.00 o "0 MS Integration Params: EVENTS.E o — Quant Time: May 2 9:54 2002 Quant Results File: 050102.RES 0 o o Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Q C Title 508 Modified GC/MS scan 3 CD Last Update Thu May 02 09:38:23 2002 3

Response via Initial Calibration Abundance TIC: 0429REFB.D

o 2200000 % 2o I O P § 2 2000000 g $o £ c CM

1g !f <> o E g8 1800000 s() ! 5 o 8 1600000 § O CM

1400000 iO zs D 5 s B O E 2 2o SB 5 o I S 1200000 21 2

1 o o s 2 6 3 CL A

8 fl o l 1 & 1 (J <£ ! 21 a§ 8 L

I 2 £ Q I 1« sIiM ill. o 1 11 Eg 1 1000000 8 GD P ET

f 800000 ll 58 g 85 §8 2 CM

2 J 1 XD N

E I h CD — 3 O

ii o

1 o w C o

600000 2 -$3s 9^ -$38 § Q

§ Q CD & CD K C Q I & 8 8 I & s I I' X w

! 3 82

I 3 Fm C o N E cm

400000 O

200000 t 09 ! | I __ ■ 1 Cp I I I « I U I I _U I I I I ■I I I I 1 I I I I 1 I I "P1 I I [ I I I I I I I I I I I __ III" | I ! I V I | I l 1 ] I । । ( | । I । । T । I I i | i TikI Time--> 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00

0429REFB.D 050102.M Thu May 02 09:54:41 2002 Page 3