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GCMS reference analysis results for sample AE10134, May 7 2002

Machine-extracted title · confidence 100%

Reference analysis report for GCMS testing of volatile organic compounds with quantified concentrations.

NYC-WTC_000044400–000044407

Folder label: “GCMS X 4/29/02 A 5/3/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\1\DATA\050202\129REF2.D Vial: 18 Acq On 3 May 2002 3:10 am Operator: Mclean Sample 4/29 ad Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 06 12:26:25 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Mon May 06 12:20:41 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

34) Anthracene 23.17 178 7928629 16.05 ug/L 98 35) Di-n-butylphthalate 25.10 149 9411465 17.74 ug/L 100 36) Fluoroanthene 26.54 202 8433115 17.03 ug/L 100 38) Pyrene 27.18 202 8850164 17.55 ug/L 99 39) Butylbenzylphthalate 29.53 149 3443702 15.33 ug/L 96 40) Benzo(a)anthracene 30.79 228 6424267 16.00 ug/L 97 41) Bis(2-ethylhexyl)phthalate 31.39 149 5713228 18.81 ug/L 96 42) Chrysene 30.89 228 7231083m 17.39 ug/L 44) Di-n-octylphthalate 33.25 149 5443734 13.84 ug/L 99 45) Benzo(b)fluoranthene 33.76 252 5579294 17.29 ug/L 96 46) Benzo(k)fluoranthene 33.83 252 7127796 17.58 ug/L 97 47) Benzo(a)pyrene 34.55 252 4582822m 14.23 ug/L 48) Indeno(1,2,3-cd)pyrene 37.40 276 2773510 12.29 ug/L 97 49) Dibenz(a,h)anthracene 37.52 278 3627720 15.11 ug/L 97 51) Benzo(g,h,i)perylene 38.14 276 3979994 15.79 ug/L 99

(#) = qualifier out of range (m) = manual integration (+) = signals summed 129REF2.D 050102.M Tue May 07 09:34:04 2002 Page 2

NYC-WTC_000044403

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NYC-WTC_000044403Source: NYC Law Department, mirrored locally

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