GCMS blank analysis results for sample AE10134, May 7 2002

NYC 9/11 Public Portal Document

• Data File C : \MSDCHEM\ 1 \DATA\ 0 5 0 2 0 2 \ 4 2 9LB . D Vial: 16 Acq On 3 May 2002 1:32 am Operator: Mclean Sample 4/29 ad Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.778 92 119 124 PV 8 6211 441013 1.24% 0.228% 2 3.820 124 126 128 W 3 5494 83288 0.23% 0.043% 3 3.849 128 131 135 W 5 5984 132524 0.37% 0.068% 4 3.890 135 138 142 W 3 5742 123412 0.35% 0.064% 5 3.966 149 151 153 W 5414 65859 0.18% 0.034%

6 4.372 212 220 225 W 8 4371 145602 0.41% 0.075% 7 5.030 326 332 340 W 6 4094 139011 0.39% 0.072% 8 5.964 485 491 514 W 276202 5194556 14.56% 2.682% 9 6.105 514 515 517 W 2 2880 25000 0.07% 0.013% 10 6.311 547 550 554 PV 4 1667 19407 0.05% 0.010%

11 6.405 564 566 568 PV 2 1679 12639 0.04% 0.007% 12 7.744 781 794 800 PV 7 3220 80846 0.23% 0.042% 13 9.936 1155 1167 1179 PV 1259974 24432202 68.50% 12.615% 14 10.012 1179 1180 1185 W 4 2271 32834 0.09% 0.017% 15 12.210 1549 1554 1565 W 4 1927 51340 0.14% 0.027%

16 12.410 1582 1588 1593 PV 9503 159983 0.45% 0.083% 17 13.432 1753 1762 1777 W 1764130 32922323 92.30% 16.998% 18 13.585 1781 1788 1793 W 2 5620 127792 0.36% 0.066% 19 15.706 2143 2149 2154 W 3 2294 36021 0.10% 0.019% 20 16.746 2317 2326 2336 W 2 3368 75346 0.21% 0.039%

21 18.127 2552 2561 2567 W 4 1600 33980 0.10% 0.018% 22 18.573 2626 2637 2648 PV 1821695 35668550 100.00% 18.416% 23 18.655 2648 2651 2655 W 2 4981 83747 0.23% 0.043% 24 18.961 2700 2703 2711 PV 2 1783 22454 0.06% 0.012% 25 20.330 2924 2936 2940 W 4 2052 54856 0.15% 0.028%

26 20.541 2957 2972 2979 PV 142829 2538503 7.12% 1.311% 27 22.580 3310 3319 3326 PV 2 12928 241691 0.68% 0.125% 28 22.956 3372 3383 3401 PV 2 1604328 34517978 96.77% 17.822% 29 23.068 3401 3402 3404 W 2 4652 52935 0.15% 0.027% 30 23.109 3404 3409 3415 W 2 ' 17188 357431 1.00% 0.185%

31 23.162 3415 3418 3433 W 7 3814 110223 0.31% 0.057% 32 29.989 4575 4580 4584 PV 3 1440 20673 0.06% 0.011% 33 30.812 4703 4720 4752 W 2 1280731 30030606 84.19% 15.505% 34 31.006 4752 4753 4756 W 4368 60709 0.17% 0.031% 35 31.035 4756 4758 4764 W 3 3020 62587 0.18% 0.032%

36 31.388 4804 4818 4848 W 2 34416 1472175 4.13% 0,760% 37 31.570 4848 4849 4855 W 4 2795 62869 0.18% 0.032%

429LB.D 050102.M Mon May 06 12:27:31 2002 Page 1

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