GCMS calibration data for method 508, April 23 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\APR2202\8757.D Vial: 13 Acq On : 22 Apr 2002 8:55 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.164 226 231 240 rBV2 15116 43339 1.13% 0.195% 2 8.183 339 342 375 rVB 330193 798106 20.84% 3.583% 3 12.213 775 781 794 rBV 1068131 2602829 67.95% 11.685% 4 14.040 976 980 987 rVB 45211 86049 2.25% 0.386% 5 15.840 1170 1176 1188 rBV 1633692 3365386 87.86% 15.109%

6 21.146 1748 1754 1767 rBV 1918481 3830542 100.00% 17.197% 7 23.285 1978 1987 1994 rVB 192191 388714 10.15% 1.745% 8 24.230 2086 2090 2095 rVB 27964 52653 1.37% 0.236% 9 24.331 2097 2101 2104 rBV2 25380 53702 1.40% 0.241% 10 24.432 2108 2112 2117 rVB 33669 62794 1.64% 0.282%

11 24.515 2117 2121 2128 rVB2 25943 51483 1.34% 0.231% 12 24.644 2128 2135 2139 rBV3 17216 51078 1.33% 0.229% 13 24.772 2145 2149 2152 rBV2 25106 57441 1.50% 0.258% 14 24.873 2157 2160 2164 rW 34860 64464 1.68% 0.289% 15 25.020 2172 2176 2179 rBV 22448 38994 1.02% 0.175%

16 25.231 2194 2199 2206 rBV3 23685 54392 1.42% 0.244% 17 25.589 2231 2238 2249 rBV 1755907 3748392 97.86% 16.828% 18 26.314 2312 2317 2321 rBV 25313 54986 1.44% 0.247% 19 27.333 2423 2428 2444 rBV 111466 300094 7.83% 1.347% 20 27.554 2448 2452 2459 rVB 42509 85373 2.23% 0.383%

21 29.270 2632 2639 2646 rVB 34462 83483 2.18% 0.375% 22 29.950 2708 2713 2717 rVB 37899 82059 2.14% 0.368% 23 32.080 2940 2945 2951 rBV 30979 63736 1.66% 0.286% 24 32.282 2962 2967 2973 rBV 23956 51314 1.34% 0.230% 25 33.640 3104 3115 3121 rBV2 1187013 2801671 73.14% 12.578%

26 33.861 3134 3139 3150 rVB 69337 166885 4.36% 0.749% 27 35.605 3324 3329 3336 rBV 14915 45263 1.18% 0.203% 28 36.688 3442 3447 3450 rBV 20181 47976 1.25% 0.215% 29 36.752 3450 3454 3461 rVB2 20425 54163 1.41% 0.243% 30 37.670 3550 3554 3565 rVB2 14128 47866 1.25% 0.215%

31 37.872 3568 3576 3592 rBV 739647 2182787 56.98% 9.799%

NYC-WTC_000044316