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GCMS calibration data for method 508, April 22 2002

Machine-extracted title · confidence 100%

Calibration data for GCMS analysis of volatile organic compounds recorded on April 22, 2002.

NYC-WTC_000044298–000044303

Folder label: “GCMS X 4/23/02 A 4/26/02

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Scanned page image, NYC-WTC_000044301
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\APR1802\7485.D Vial: 18 Acq On : 20 Apr 2002 10:09 am Operator: Sample : gc/ms scan 4/1 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.213 775 781 797 rVB 868838 2124217 67.89% 13.935% 2 15.848 1171 1177 1189 rBV 1294537 2737759 87.50% 17.960% 3 21.145 1748 1754 1768 rBV 1582408 3128992 100.00% 20.527% 4 23.284 1979 1987 1992 rBV 142556 276057 8.82% 1.811% 5 25.588 2231 2238 2248 rBV 1455462 3035620 97.02% 19.915%

6 33.640 3105 3115 3121 rBV2 1018311 2252272 71.98% 14.776% 7 37.872 3568 3576 3596 rBV2 582823 1688325 53.96% 11.076%

Sum of corrected areas: 15243242

7485 .D GCMS0419.M Mon Apr 22 12:35:26 2002

NYC-WTC_000044301

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NYC-WTC_000044301Source: NYC Law Department, mirrored locally

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