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GCMS analysis results for sample AE10021, May 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE10021 conducted on May 14, 2002, identifying unknown compounds.

NYC-WTC_000044144–000044155

Folder label: “GCMS X 4/26/02 A 5/8/02

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NYC 9/11 Public Portal Document LatloI Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\020507\10021.D Vial: 20 Acq On 8 May 2002 6:51 am Operator: Nefliu Sample sample Inst Instrumen Mise . Multiplr: 1.00 MS Integration Params: Iscint.e Quant Time: May 09 09:46:10 2002 Quant Results File: SCAN020507.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Thu May 09 09:21:01 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.38 152 529336 40.00 ug/1 -0.01 10) Naphthalene-d8 16.53 136 1988192 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.46 164 1070131 40.00 ug/1 -0.02 30) Phenanthrene-dlO 31.72 188 1842441 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 1489071 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 1009421 40.00 ug/1 -0.03 System Monitoring Compounds 2 7) TCMX 27.54 207 70749 8.28 ug/1 -0.04 Spiked Amount 10.000 Recovery = 82.80% Target Compounds Qvalue 43) Bis(2-ethylhexyl)phthalate 40.52 149 62494 1.96 ug/1 98

(#) = qualifier out of range (m) = manual) integration ( + ) = signals summed L0021.D SCAN020507.M Thu May 09 09:48:01' 2002 Page 1

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NYC-WTC_000044146

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NYC-WTC_000044146Source: NYC Law Department, mirrored locally

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