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GC/MS analysis results, sample AE09767, May 2002

Machine-extracted title · confidence 90%

Analytical report for sample AE09767 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.

NYC-WTC_000043779–000043791

Folder label: “GCMS X 4/25/02 A 5/7/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\020507\09767 .D Vial: 14 Acq On 8 May 2002 12:57 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: Iscint.e Quant Time: May 09 09:32:25 2002 Quant Results File: SCAN020507.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Thu May 09 09:21:01 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.38 152 498640 40.00 ug/1 -0.01 10) Naphthalene-d8 16.53 136 1891404 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.46 164 1005924 40.00 ug/1 -0.02 30) Phenanthrene-dlO 31.72 188 1731144 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 1394908 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 919722 40.00 ug/1 -0.03

System Monitoring Compounds 27) TCMX 27.54 207 61251 7.62 ug/1 -0.04 Spiked Amount 10.000 Recovery = 76.20%

Target Compounds Qvalue 43) Bis(2-ethylhexyl)phthalate 40.52 149 10900 0.36 ug/1 90

(#) = qualifier out of range (m) = manual integration (+) = signals summed 09767.D SCAN020507.M Thu May 09 09:34:40 2002 Page 1

NYC-WTC_000043781

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NYC-WTC_000043781Source: NYC Law Department, mirrored locally

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