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GCMS reference standard results, sample AE09771, May 2002

Machine-extracted title · confidence 100%

Reference analysis report for sample AE09771 confirming expected concentrations of target compounds from May 8, 2002.

NYC-WTC_000043885–000043892

Folder label: “GCMS X 4/25/02 A 5/7/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\050602\0425REFB.D Vial: 18 Acq On 7 May 2002 1:33 am Operator: Mclean Sample 4/25 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 07 15:41:38 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chernstation Integrator) Title : 508 Modified GC/MS scan Last Update : Tue May 07 14:35:08 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

34) Anthracene 23.17 178 7240698 14.80 ug/L 98 35) Di-n-butylphthalate 25.09 149 8573078 16.33 ug/L 99 36) Fluoroanthene 26.54 202 7807100 15.93 ug/L 99 3 8) Pyrene 27.17 202 8148118 16.21 ug/L 98 39) Butylbenzylphthalate 29.53 149 2990716 13.36 ug/L # 96 40) Benzo(a)anthracene 30.79 228 5729415 14.32 ug/L 97 41) Bis(2-ethylhexyl)phthalate 31.39 149 3915540 12.94 ug/L 97 42) Chrysene 30.88 228 6676463m 16.12 ug/L 44) Di-n-octylphthalate 33.24 149 4010994 10.43 ug/L 100 45) Benzo(b)fluoranthene 33.75 252 4776653 15.15 ug/L 97 46) Benzo(k)fluoranthene 33.82 252 6628001 16.73 ug/L 98 47) Benzo(a)pyrene 34.55 252 3570971m 11.35 ug/L 48) Indeno(1,2,3-cd)pyrene 37.39 276 1932329 8.76 ug/L 98 49) Dibenz(a,h)anthracene 37.51 278 2517029 10.73 ug/L 100 51) Benzo(g,h,i)perylene 38.13 276 3460329m 14.05 ug/L

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0425REFB.D 050102.M Tue May 07 15:42:32 2002 Page 2

NYC-WTC_000043891

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NYC-WTC_000043891Source: NYC Law Department, mirrored locally

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