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GC/MS analysis results, sample AE09768, May 2002

Machine-extracted title · confidence 90%

Analytical report for sample AE09768 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.

NYC-WTC_000043792–000043805

Folder label: “GCMS X 4/25/02 A 5/7/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File C:\MSDCHEM\l\DATA\020507\09768.D Vial: 15 Acq On 8 May 2002 1:56 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 0.7 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.349 41 46 52 rBV 26716 32200 0.73% 0.131% 2 3.649 90 97 108 rBV2 32189 50369 1.15% 0.206% 3 6.123 512 518 520 rBV 46466 69620 1.58% 0.284% 4 6.152 520 523 561 rVB 572499 1138257 25.89% 4.645% 5 11.375 1401 1412 1430 rBV 1257544 3120379 70.98% 12.734%

6 15.459 2094 2107 2117 rBV2 55796 155938 3.55% 0.636% 7 16.534 2275 2290 2307 rBV 1525994 3946235 89.76% 16.104% 8 24.460 3620 3639 3655 rBV2 1466415 4080885 92.83% 16.653% 9 27.539 4146 4163 4178 rBV2 197391 543596 12.36% 2.218% 10 31.082 4758 4766 4778 rVB5 11442 35325 0.80% 0.144%

11 31.717 4857 4874 4896 rBV2 1477089 4396284 100.00% 17.941% 12 31.952 4904 4914 4922 rBV2 13913 38898 0.88% 0.159% 13 39.931 6261 6272 6291 rBV2 2036223 3906771 88.87% 15.943% 14 40.518 6366 6372 6385 rVB3 28685 80120 1.82% 0.327% 15 43.151 6809 6820 6845 rBV2 1417980 2909832 66.19% 11.875%

Sum of corrected areas: 24504709

09768.D SCAN020507 .M Tue May 14 08:42:47 2002 Page 1

NYC-WTC_000043796

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NYC-WTC_000043796Source: NYC Law Department, mirrored locally

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