GCMS chain of custody form, sample AE10236, May 2002

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File C:\MSDCHEM\l\DATA\020509\10236.D Vial: 14 Acq On 9 May 2002 11:28 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 0.7 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 6.152 517 523 565 rBV 604557 1218659 23.90% 4.349% 2 11.088 1358 1363 1378 rBV5 13624 58169 1.14% 0.208% 3 11.205 1378 1383 1399 rW4 16187 59432 1.17% 0.212% 4 11.376 1400 1412 1432 rVB 1410651 3612187 70.83% 12.892% 5 11.523 1432 1437 1457 rBV2 29563 114371 2.24% 0.408%

6 16.534 2273 2290 2305 rBV 1737080 4595107 90.11% 16.400% 7 24.461 3619 3639 3654 rBV2 1690762 4804067 94.21% 17.146% 8 27.539 4147 4163 4174 rBV3 245436 697632 13.68% 2.490% 9 31.088 4755 4767 4777 rVB5 14161 43790 0.86% 0.156% 10 31.717 4856 4874 4895 rBV4 1620906 5099510 100.00% 18.200%

11 31.952 4904 4914 4923 rVB4 15923 46164 0.91% 0.165% 12 39.931 6258 6272 6292 rBV2 2167182 4423260 86.74% 15.787% 13 40.518 6366 6372 6383 rBV5 14072 37625 0.74% 0.134% 14 43.151 6808 6820 6843 rBV2 1512008 3208804 62.92% 11.452%

Sum of corrected areas: 28018777

10236.D SCAN020507.M Tue May 14 14:23:44 2002 Page 1

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