Calibration data sheet listing retention times and response factors for deuterated internal standards used in TCLP testing.
NYC-WTC_000043378–000043384Folder label: “GCMS X 4/23/02 A 4/24/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\APR1802\7002.D Vial: 20 Acq On : 19 Apr 2002 6:30 am Operator : Sample : GC/MS SCAN 3/26 FB Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 19 15:04 2002 (Quant Results File: GCMS0419.RES > Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) • Title : 209 625/TCLP calibration table Last Update Response via DataAcq Meth : : : Fri Apr 19 14:51:24 2002 Initial Calibration GCMS0412 6 Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.21 152 635528 20.00 ug/1 -0.03 10) Naphthalene-d8 15.85 136 2328604 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.15 164 1293858 20.00 ug/1 -0.02 30) Phenanthrene-diO 25.59 188 1878770 20.00 ug/1 -0.03 39) Chrysene-dl2 33.65 240 1200041 20.00 ug/1 -0.03 45) Perylene-dl2 37.87 264 763420 20.00 ug/1 -0.05
System Monitoring Compounds 2 8) TCMX 23.28 209 34233 3.17 ug/L -0.05 Spiked Amount 4.000 Recovery = 79.25% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.49 165 100 N.D. 25) Diethylphthalate 22.63 149 730 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D.
(#) = qualifier out of range (m) = manual integration 7002.D GCMS0419.M Fri Apr 19 15:05:58 2002 Page 1
NYC-WTC_000043378
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Gas chromatography-mass spectrometry analysis report for sample AE07107 including surrogate compound recovery data.
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Technical document displaying GCMS calibration data and compound retention times for sample AE09448 processed in early May 2002.
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Technical document displaying GCMS calibration data and compound retention times for sample AE09447 processed in early May 2002.
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Gas chromatography-mass spectrometry analysis report for sample AE07067 including surrogate compound recovery data.
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Reviewed data file listing retention times and response factors for deuterated internal standards.
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Reviewed data file listing retention times and response factors for deuterated internal standards.
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Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.
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Laboratory report of GCMS analysis for sample AE10063 conducted on May 23, 2002, showing surrogate recovery data.
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Laboratory report of GCMS analysis for sample AE10065 conducted on May 23, 2002, showing surrogate recovery data.
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Laboratory report of GCMS analysis for sample AE10062 conducted on May 23, 2002, showing surrogate recovery data.
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