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Document / 7 pages

TCLP calibration table review document, April 2002

Machine-extracted title · confidence 100%

Calibration data sheet listing retention times and response factors for deuterated internal standards used in TCLP testing.

NYC-WTC_000043362–000043368

Folder label: “GCMS X 4/23/02 A 4/24/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APRI802\7001.D Vial: 19 Acq On : 19 Apr 2002 5:32 am Operator: Sample : GC/MS SCAN 3/26 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 19 15:02 2002 Quant Results File: GCMS0419.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Apr 19 14:51:24 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.65 178 559 N.D. 35) Anthracene 25.78 178 226 N.D. 36) Di-n-butylphthalate 27.55 149 2882 N.D. 37) Fluoranthene 29.26 202 308 N.D. 40) Pyrene 29.96 202 425 N.D. 41) Butylbenzylphthalate 32.07 149 190 N.D. 42) Benzo(a)anthracene 33.64 228 4262 N.D. 43) Bis(2-ethylhexyl)phthalate 33.86 149 13612 0.42 ug/1 # 97 44) Chrysene 33.70 228 1786 N.D. 46) Di-n-Octylphthalate 35.60 149 190 N.D. 47) Benzo(b)fluoranthene 36.68 252 876 N.D. 48) Benzo(k)fluoranthene 36.75 252 833 N.D. 49) Benzo(a)pyrene 37.66 252 189 N.D. 50) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 51) Dibenz(a,h)anthracene 0.00 278 0 N.D. 52) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 7001.D GCMS0419.M Fri Apr 19 15:04:23 2002 Page 2

NYC-WTC_000043363

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NYC-WTC_000043363Source: NYC Law Department, mirrored locally

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