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ICPMS daily performance check report, April 23, 2002

Machine-extracted title · confidence 95%

Daily instrument performance verification log for ICPMS analysis including intensity and standard deviation data for multiple elements.

NYC-WTC_000040976–000041063

Folder label: “ICPMS 4/23/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE08932 Sample Date/Time: Tuesday, April 23, 2002 10:37:59 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: d:\elandata\Method\NYC.mth Dataset File: d:\elandata\Dataset\nevy york city\AE08932.670 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas, intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 7.333 34.317 -0.000 -0.00497 145.27 ug/L Se-1 45 467059.202 0.848 467059.202 ug/L Cr 52 10731.104 1.291 0.007 0.39662 5.97 ug/L Cr 53 1401.122 2.443 0.001 0.66156 5.98 ug/L Mn 55 237741.214 0.202 0.507 17.90939 0.94 ug/L Ni 60 1074.408 3.670 0.002 0.41106 3.61 ug/L Cu 63 29071.048 2.306 0.061 5.98398 2.35 ug/L Cu 65 14278.353 2.879 0.030 5.87858 3.31 ug/L Zn 66 5698.843 0.123 0.054 3.22489 1.32 ug/L Zn 67 1119.747 2.617 0.010 3.40545 4.24 ug/L Zn 68 4786.641 1.291 0.046 3.66799 2.60 ug/L > Ge 72 91714.597 1.098 91714.597 ug/L As 75 807.741 3.687 0.008 0.41970 3.03 ug/L Se 77 168.199 9.728 0.001 0.34589 26.62 ug/L Se 82 147.669 7.460 0,000 0.20762 23.61 ug/L Ag 107 182.337 11.271 -0.000 -0.04557 4.88 ug/L Cd 111 928.846 3.363 -0.000 -0.03393 39.77 ug/L Cd 114 -34.914 1068.884 -0.000 -0.03118 204.50 ug/L In 115 1248896.379 0.267 1248896.379 ug/L Sb 121 625.029 33.700 0.000 0.06810 36.19 ug/L Sb 123 412.287 4.739 0.000 0.05688 5.05 ug/L Ba 135 41547.811 0.850 0.024 16.51309 1.13 ug/L Ba 137 72704.705 2.007 0.042 16.50131 0.72 ug/L > Tb 159 1714885.185 1.300 1714885.185 ug/L Ho 165 1703435.354 0.927 0.002 ug/L Hg 201 50.667 16.075 -0.000 -0.00307 257.42 ug/L Hg 202 107.335 13.220 -0.000 -0.00983 53.60 ug/L TI 205 745.038 6.511 0.000 0.00383 47.02 ug/L Pb 208 4562.492 2.280 0.002 0.08859 1.93 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ' Be 9 > Sc-1 45 100.582 Cr 52

Sample ID: AE08932 Report Date/Time: Tuesday, April 23, 2002 10:39:52 Page 1

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NYC-WTC_000041028Source: NYC Law Department, mirrored locally

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