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ICPMS daily performance check report, April 23, 2002

Machine-extracted title · confidence 95%

Daily instrument performance verification log for ICPMS analysis including intensity and standard deviation data for multiple elements.

NYC-WTC_000040976–000041063

Folder label: “ICPMS 4/23/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE08839 Sample Date/Time: Tuesday, April 23, 2002 10:18:29 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: d:\elandata\Method\NYC.mth Dataset File: d:\elandata\Dataset\new york city\AE08839.665 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 7.667 39.849 -0.000 -0.00458 184.93 ug/L > Se-1 45 478894.285 0.630 478894.285 ug/L Cr 52 9901.489 1.470 0.005 0.27037 4.03 ug/L Cr 53 1171.087 7.352 0.001 0.40544 19.66 ug/L Mn 55 251704.381 2.957 0.524 18.49688 3.60 ug/L Ni 60 996.731 7.766 0.002 0.36265 10.73 ug/L Cu 63 31939.665 0.988 0.066 6.41863 1.03 ug/L Cu 65 15709.723 2.086 0.032 6.31537 2.65 ug/L Zn 66 2901.826 2.033 0.022 1.34904 2.09 ug/L Zn 67 682.699 5.037 0.005 1.78301 6.68 ug/L Zn 68 2748.110 2.901 0.023 1.82716 3.36 ug/L > Ge 72 93810.143 0.514 93810.143 ug/L As 75 928.868 8.811 0.009 0.47547 9.00 ug/L Se 77 173.525 4.226 0.001 0.35515 11.07 ug/L Se 82 159.003 9.136 0.001 0.24702 27.79 ug/L Ag 107 111.335 7.260 -0.000 -0.05333 1.92 ug/L Cd 111 954.814 6.517 -0.000 -0.03284 60.23 ug/L Cd 114 220.924 20.775 0.000 0.01173 ’ 69.52 ug/L In 115 1279501.622 1.642 1279501.622 ug/L Sb 121 431.681 8.931 0.000 0.04411 8.66 ug/L Sb 123 335.992 5.367 0.000 0.04411 7.91 ug/L Ba 135 42800.280 0.799 0.024 16.40973 0.23 ug/L Ba 137 74313.259 0.987 0.042 16.27283 1.15 ug/L > Tb 159 1777583.280 1.029 1777583.280 ug/L Ho 165 1759634.187 0.879 -0.002 ug/L Hg 201 51.667 17.562 -0.000 -0.00393 195.28 ug/L Hg 202 110.668 6.151 -0.000 -0.01004 22.04 ug/L TI 205 789.376 1.833 0.000 0.00456 11.97 ug/L Pb 208 9038.172 0.067 0.004 0.22338 1.23 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ' Be 9 > Sc-1 45 103.130 Cr 52

Sample ID: AE08839 Report Date/Time: Tuesday, April 23, 2002 10:21:07 Page 1

NYC-WTC_000041013

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NYC-WTC_000041013Source: NYC Law Department, mirrored locally

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