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ICPMS daily performance check report, April 23, 2002

Machine-extracted title · confidence 95%

Daily instrument performance verification log for ICPMS analysis including intensity and standard deviation data for multiple elements.

NYC-WTC_000040976–000041063

Folder label: “ICPMS 4/23/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE08839 Sample Date/Time: Tuesday, April 23, 2002 10:14:18 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: d:\elandata\Method\NYC.mth Dataset File: d:\elandata\Dataset\new york city\AE08839.664 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 \ 8.333 24.980 -0.000 -0.00228 273.03 ug/L > Se-1 45 472183.402 1.896 472133.402 ug/L Cr 52 10734.443 2.307 0,007 0.38331 2.67 ug/L Cr 53 1177.421 3.809 9.001 0.42829 12.07 ug/L Mn 55 249867.536 0.666 /0.527 18.62738 2.15 ug/L Ni 60 20845.751 1.578 / 0.044 9.70768 0.65 ug/L Cu 63 31804.872 2.132 / 0.066 6.48481 2.26 ug/L Cu 65 16004.571 1.453 / 0.033 6.53012 2.15 ug/L Zn 66 3855.523 1.395 / 0.033 2.00522 1.82 ug/L Zn 67 799.376 3.263 / 0.007 2.24307 4.13 ug/L Zn 68 3394.001 3.608 \ / 0.030 2.43348 4.16 ug/L > Ge 72 92130.068 0.191 / \ 92130.068 ug/L As 75 821.184 5.673 / \ 0.008 0.42515 5.87 ug/L Se 77 161.462 \ 0.001 0.30075 25.02 ug/L Se 82 157.670 4.223 0.001 0.25476 12.76 ug/L Ag 107 113.669 7.482 -0000 -0.05322 1.80 ug/L Cd 111 1042.902 2.575 -0.000 -0.00203 704.18 ug/L Cd 114 350.675 23.501 0.000 0.03277 43.12 ug/L > In 115 1292638.399 .093 1292638.399 ug/L Sb 121 440.348 / 2.803 0.000 0.04463 3.58 ug/L Sb 123 344.077 7 1.421 0.000 604475 0.51 ug/L Ba 135 42700.505 2.158 0.024 16.12082 1.79 ug/L Ba 137 74717.885 0.772 0.041 16.11158 0.84 ug/L > Tb 159 1805096.821 0.983 1805096.821 ug/L Ho 165 1766358.880 1.415 -0.013 ug/L Hg 201 76.668 0.753 0.000 0.01739 3.73 ug/L Hg 202 175.670 10.761 0.000 0.01378 46.99 ug/L 71 205 820.712 11.102 0.000 0.00536 72.61 ug/L Pb 208 12021.543 0.569 0.006 0.31097 1.49 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ’ Be 9 > Sc-1 45 101.674 Cr 52

Sample ID: AE08839 Report Date/Time: Tuesday, April 23, 2002 10:16:11 Page 1

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NYC-WTC_000041010Source: NYC Law Department, mirrored locally

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