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ICPMS daily performance check report, April 23, 2002

Machine-extracted title · confidence 95%

Daily instrument performance verification log for ICPMS analysis including intensity and standard deviation data for multiple elements.

NYC-WTC_000040976–000041063

Folder label: “ICPMS 4/23/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: ICV CALBK Sample Date/Time: Tuesday, April 23, 2002 09:24:53 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: d:\elandata\Method\NYC.mth Dataset File: d:\elandata\Dataset\new york cit\ICV CAL BK.656 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 9.000 44.444 -0.000 -0.00039 2928.73 ug/L Se-1 45 472439.562 2.270 472439.562 ug/L Cr 52 7058.143 1.032 -0.001 -0.04391 23.31 ug/L Cr 53 665.698 4.742 -0.000 -0.07284 22.43 ug/L Mn 55 865.383 9.028 -0.000 -0.00899 52.43 ug/L Ni 60 210.338 9.321 -0.000 -0.00078 1429.53 ug/L Cu 63 415.014 5.060 -0.000 -0.00818 33.27 ug/L Cu 65 220.005 7.144 -0.000 -0.01002 58.33 ug/L Zn 66 712.369 17.200 -0.001 -0.03517 235.55 ug/L Zn 67 138.336 7.730 -0.000 -0.10534 37.92 ug/L Zn 68 547.689 16.935 -0.000 -0.03881 216.10 ug/L > Ge 72 90186.708 0.236 90186.708 ug/L As 75 63.726 67.927 0.000 0.00685 356.49 ug/L Se 77 109.217 19.264 -0.000 -0.00358 3665.66 ug/L Se 82 104.002 7.510 -0.000 -0.00360 1083.18 ug/L Ag 107 2397.010 12.549 0.001 0.17767 16.00 ug/L Cd 111 984.585 4.424 -0.000 -0.02763 73.72 ug/L Cd 114 125.321 16.559 -0.000 -0.00460 77.83 ug/L > In 115 1302315.641 0.905 1302315.641 ug/L Sb 121 55.334 13.564 0.000 0.00077 103.06 ug/L Sb 123 51.656 25.628 0.000 0.00174 106.70 ug/L Ba 135 79.334 5.684 -0.000 -0.00245 83.74 ug/L Ba 137 132.669 1.569 -0.000 -0.00035 228.21 ug/L > Tb 159 1824618.367 1.505 1824618.367 ug/L Ho 165 1805303.765 1.274 -0.002 ug/L Hg 201 104.335 13.868 0.000 0.04061 27.41 ug/L Hg 202 210.338 7.582 0.000 0.02599 18.35 ug/L TI 205 756.372 2.568 0.000 0.00236 21.98 ug/L Pb 208 1806.421 2.773 -0.000 -0.00428 /16.55 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 > Sc-1 45 101.740 Cr 52

Sample ID: ICV CALBK Report Date/Time: Tuesday, April 23, 2002 09:27:25 Page 1

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