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ICPMS daily performance check report, April 22, 2002

Machine-extracted title · confidence 95%

Daily instrument performance verification log for ICPMS analysis including intensity and standard deviation data for multiple elements.

NYC-WTC_000040871–000040923

Folder label: “ICPMS 4/22/01

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE08481 Sample Date/Time: Monday, April 22, 2002 12:45:45 Sample Type: Spike -1 Sample Description: Number of Replicates: 3 Method File: d:\elandata\Method\NEWQ200.8.mth Dataset File: d:\elandata\Dataset\NEWQ\NEWQ\AE08481.503 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 18382.418 0.777 0.038 55.37985 0.81 ug/L Se-1 45 486368.261 0.137 486368.261 ug/L Cr 52 444857.576 0.408 0.898 48.40012 0.30 ug/L Cr 53 52861.443 0.799 0.107 47.88389 0.72 ug/L Mn 55 911038.289 1.709 1.869 64.63740 1.64 ug/L Ni 60 110936.650 1.530 0.228 47.25052 - 1.62 ug/L Cu 63 254453.152 0.563 0.522 47.62357 0.45 ug/L Cu 65 125506.849 1.799 0.258 47.43361 1.67 ug/L Zn 66 91285.268 0.188 0.961 57.52982 0.98 ug/L Zn 67 16089.390 2.114 0.169 55.37161 2.45 ug/L Zn 68 68547.142 0.231 0.722 57.57107 0.84 ug/L > Ge 72 94240.576 0.792 94240.576 ug/L As 75 98587.038 0.522 1.045 52.18345 0.31 ug/L Se 77 9902.355 1.226 0.104 57.87164 1.07 ug/L Se 82 11731.349 1.385 0.123 56.73535 0.60 ug/L Ag 107 498271.100 0.302 0.379 48.99142 0.69 ug/L > In 115 1314667.171 0.993 1314667.171 ug/L Sb 121 454036.399 1.200 0.345 52.15563 0.58 ug/L Sb 123 354200.048 0.655 0.269 52.46652 0.35 ug/L Ba 135 177019.466 1.306 0.097 65.69312 1.06 ug/L • Ba 137 310304.558 0.670 0.170 66.23703 0.28 ug/L Ho 165 1819906.470 1.189 0.005 ug/L > Tb 159 1827246.971 0.879 1827246.971 ug/L Hg 201 4762.962 1.305 0.003 3.90747 1.75 ug/L Hg 202 11056.497 0.789 0.006 4.06785 1.55 ug/L TI 205 1220314.308 0.500 0.667 48.69585 0.44 ug/L Pb 208 1634087.183 0.633 0.893 48.38659 0.62 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ' Be 9 110.787 > Sc-1 45 114.606 Cr 52 96.268 Cr 53 95.188 Mn 55 96.130

Sample ID: AE08481 Report Date/Time: Monday, April 22, 2002 12:48:08 Page 1

NYC-WTC_000040896

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