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ICPMS daily performance check report, April 16, 2002

Machine-extracted title · confidence 95%

Daily instrument performance verification log for ICPMS analysis including intensity and standard deviation data for multiple elements.

NYC-WTC_000040755–000040869

Folder label: “ICPMS 4/16/02”

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Scanned page image, NYC-WTC_000040830
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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE07959 NO NYC Sample Date/Time: Tuesday, April 16, 2002 13:28:37 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: d:\elandata\Method\NYC.mth Dataset File: d:\elandata\Dataset\new york city\AE07959 NO NYC.583 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 9.667 46.647 -0.000 -0.00767 129.59 ug/L > Se-1 45 531276.300 3.436 531276.300 ug/L Cr 52 26992.290 1.729 0.034 1.76278 6.99 ug/L Cr 53 1898.217 1.378 0.002 0.97712 6.85 ug/L Mn 55 3635.430 1.211 0.004 0.14414 7.07 ug/L Ni 60 1890.549 2.159 0.003 0.71157 2.87 ug/L Cu 63 69526.007 2.732 0.130 12.33312 1.16 ug/L Cu 65 33530.770 3.307 0.063 11.36189 6.72 ug/L Zn 66 38562.702 2.505 0.407 22.51948 0.22 ug/L Zn 67 5850.608 1.936 0.061 18.70600 1.18 ug/L Zn 68 29670.306 1.171 0.313 23.56603 3.51 ug/L > Ge 72 93503.170 2.369 93503.170 ug/L As 75 141.569 53.972 0.001 0.06211 63.25 ug/L Se 77 200.263 6.234 0.001 0.57261 8.59 ug/L Se 82 175.337 14.136 0.001 0.34463 34.16 ug/L Ag 107 3789.162 5.344 0.003 0.33322 6.95 ug/L Cd 111 796.085 0.513 -0.000 -0.07831 1.79 ug/L Cd 114 99.782 24.512 -0.000 -0.00588 73.91 ug/L > In 115 1234054.175 0.959 1234054.175 ug/L Sb 121 110.335 8.224 0.000 0.00895 11.09 ug/L Sb 123 79.856 8.036 0.000 0.00652 15.34 ug/L Ba 135 4418.451 1.629 0.003 1.73357 1.08 ug/L Ba 137 7890.836 1.037 0.005 1.75566 2.52 ug/L > Tb 159 1665745.529 2.001 1665745.529 ug/L Ho 165 1715889.867 2.289 0.054 ug/L n 205 1159.419 4.524 -0.000 -0.01952 8.08 ug/L Pb 208 14816.146 1.841 0.008 0.41526 1.79 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ' Be 9 > Sc-1 45 108.704 Cr 52 Cr 53 Mn 55

Sample ID: AE07959 NO NYC Report Date/Time: Tuesday, April 16, 2002 13:30:24 Page 1

NYC-WTC_000040830

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NYC-WTC_000040830Source: NYC Law Department, mirrored locally

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