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ICPMS daily performance check report, April 16, 2002

Machine-extracted title · confidence 95%

Daily instrument performance verification log for ICPMS analysis including intensity and standard deviation data for multiple elements.

NYC-WTC_000040755–000040869

Folder label: “ICPMS 4/16/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: LRB Sample Date/Time: Tuesday, April 16, 2002 09:45:16 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: d:\elandata\Method\NYC.mth Dataset File: d:\elandata\Dataset\new york cit\LRB.554 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 12.000 30.046 -0.000 -0.00062 1385.00 ug/L > Se-1 45 498882.288 0.692 498882.288 ug/L Cr 52 7979.915 1.720 -0.001 -0.05060 39.34 ug/L Cr 53 562.023 2.446 -0.000 -0.10021 15.55 ug/L Mn 55 1266.101 4.480 0.000 0.00362 102.24 ug/L Ni 60 46.334 5.432 0.000 0.00002 4406.52 ug/L Cu 63 256.340 2.508 -0.000 -0.00268 55.98 ug/L Cu 65 149.669 11.067 0.000 0.00021 2701.20 ug/L Zn 66 505.019 6.224 -0.000 -0.01718 100.86 ug/L Zn 67 114.669 13.120 -0.000 -0.06954 74.28 ug/L Zn 68 370.678 5.788 ■0.000 -0.03013 65.15 ug/L Ge 72 97447.857 1.255 97447.857 ug/L As 75 6.049 1420.368 -0.000 -0.00692 610.31 ug/L Se 77 110.032 18.475 0.000 0.03612 311.92 ug/L Se 82 99.668 16.064 -0.000 -0.03021 253.23 ug/L Ag 107 1990.260 39.277 0.001 0.13748 47.99 ug/L Cd 111 1081.818 2.186 -0.000 -0.00995 104.95 ug/L Cd 114 95.444 16.850 -0.000 -0.00834 27.46 ug/L > In 115 1374991.529 1.270 1374991.529 ug/L Sb 121 81.335 19.453 0.000 0.00443 37.33 ug/L Sb 123 63.856 25.655 0.000 0.00311 70.79 ug/L Ba 135 64.668 3.571 0.000 0.00132 68.72 ug/L Ba 137 104.335 17.047 0.000 0.00273 133.35 ug/L Tb 159 1861362.139 0.497 1861362.139 ug/L Ho 165 1823655.480 2.826 0.004 ug/L TI 205 1989.905 7.842 0.000 0.00893 67.25 ug/L Pb 208 1959.103 2.726 -0.000 -0.01232 13.95 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ’ Be 9 > Se-1 45 102.076 Cr 52 Cr 53 Mn 55

Sample ID: LRB Report Date/Time: Tuesday, April 16,2002 09:50:57 Page 1

NYC-WTC_000040772

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