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ICPMS daily performance check report, April 11, 2002

Machine-extracted title · confidence 95%

Daily instrument performance verification log for ICPMS analysis including intensity and standard deviation data for multiple elements.

NYC-WTC_000040598–000040646

Folder label: “ICPMS 4/11/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: ICV STD1 30 PPB Sample Date/Time: Thursday, April 11, 2002 12:40:17 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: d:\elandata\Method\NYC.mth Dataset File: d:\elandata Datasetinew york cityICV STD1 30PPB.468 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 12898.277 2.584 0.027 30.34642 4.82 ug/L . Se-1 45 486337.566 2.206 486337.566 ug/L Cr 52 263121.670 1.545 0.526 29.27048 3.77 ug/L Cr 53 30956.614 2.435 0.063 28.41172 0.25 ug/L Mn 55 440085.052 3.698 0.902 30.15238 5.23 ug/L NI 60 62799.881 2.523 0.129 29.56259 4.43 ug/L Cu 63 152295.705 1.213 0.313 29.82692 1.81 ug/L Cu 65 70228.010 2.311 0.144 28.83281 4.54 ug/L Zn 66 46979.929 2.463 0.489 28.03072 3.79 ug/L Zn 67 8653.539 2.859 0.090 29.62389 2.20 ug/L Zn 68 34720.875 1.974 0.361 29.44034 1.88 ug/L Ge 72 94473.685 1.358 94473.685 ug/L As 75 52843.580 2.507 0.559 28.70585 1.96 ug/L Se 77 4788.976 2.775 0.050 29.17702 4.11 ug/L Se 82 6129.794 1.487 0.064 29.47826 2.33 ug/L Ag 107 289451.925 0.928 0.223 28.86768 1.10 ug/L Cd 111 79691.373 3.652 0.061 30.36006 2.02 ug/L Cd 114 184911.670 1.803 0.143 30.15291 3.46 ug/L > in 115 1288761.538 1.667 1288761.538 ug/L Sb 121 272064.983 0.996 0.211 30.31192 1.98 ug/L Sb 123 202146.069 2.755 0.157 30.15954 1.09 ug/L Ba 135 77810.075 1.652 0.043 30.19091 0.75 ug/L Ba 137 129702.128 1.566 0.072 29.21996 1.75 ug/L > Tb 159 1793346.070 0.947 1793346.070 ug/L Ho 165 1714311.957 2.249 -0.005 ug/L TI 205 740257.240 1.126 0.412 30.61235 2.07 ug/L Pb 208 989336.519 1.155 0.551 30.22432 0.76 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ' Be 9 > Sc-1 45 102.507 Cr 52 Cr 53 Mn 55

Sample ID: ICV STD1 30PPB Report Date/Time: Thursday, April 11, 2002 12:42:36 Page 1

NYC-WTC_000040607

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NYC-WTC_000040607Source: NYC Law Department, mirrored locally

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