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ICPMS daily performance check report, April 10, 2002

Machine-extracted title · confidence 95%

Daily instrument performance verification log for ICPMS analysis including intensity and standard deviation data for multiple elements.

NYC-WTC_000040452–000040596

Folder label: “ICPMS 4/10/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE07766 Sample Date/Time: Wednesday, April 10, 2002 12:30:10 Sample Type: Spike -1 Sample Description: MSD Number of Replicates: 3 Method File: d:\elandata\Method\NEWQ200.8.mth Dataset File: d:\elandata\Dataset\NEWQ\NEWQ\AE07766.461 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 22770.043 0.897 0.049 52.84866 1.52 ug/L Se-1 45 467919.307 1.187 467919.307 ug/L Cr 52 432535.750 0.507 0.911 49.61518 0.72 ug/L Cr 53 52028.649 0.683 0.110 50.65961 0.51 ug/L Mn 55 902902.207 1.912 1.925 65.38037 2.41 ug/L Ni 60 105091.668 0.579 0.225 48.82220 0.96 ug/L Cu 63 243198.586 0.753 0.519 49.00399 1.63 ug/L Cu 65 119850.150 1.460 0.256 49.54494 2.35 ug/L Zn 66 82544.207 0.190 0.887 51.25323 2.53 ug/L Zn 67 14702.362 1.682 0.158 51.49310 2.11 ug/L Zn 68 61488.284 2.615 0.660 51.87777 0.59 ug/L > Ge 72 92238.357 2.544 92238.357 ug/L As 75 95225.225 2.043 1.029 51.37556 1.36 ug/L Se 77 8383.281 1.620 0.090 53.22632 3.31 ug/L Se 82 11272.097 0.242 0.120 53.11073 2.66 ug/L Ag 107 479233.957 1.185 0.386 47.63074 1.94 ug/L > In 115 1241166.349 0.772 1241166.349 ug/L Sb 121 441306.767 0.642 0.356 52.51493 1.38 ug/L Sb 123 338859.619 1.176 0.273 51.91385 1.45 ug/L Ba 135 161920.768 1.520 0.094 62.63628 1.39 ug/L Ba 137 281352.015 0.806 0.163 62.44077 0.97 ug/L Ho 165 1716115.769 0.883 0.133 ug/L > Tb 159 1728568.501 0.471 1728568.501 ug/L TI 205 1146763.597 0.313 0.663 48.11562 0.55 ug/L Pb 208 1548132.190 1.252 0.895 47.96067 0.85 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ' Be 9 105.701 > Sc-1 45 83.176 Cr 52 98.431 Cr 53 100.661 Mn 55 98.367 NI 60 96.970 Cu 63 96.170

Sample ID: AE07766 Report Date/Time: Wednesday, April 10, 2002 12:32:18 Page 1

NYC-WTC_000040537

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NYC-WTC_000040537Source: NYC Law Department, mirrored locally

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