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ICPMS daily performance check report, April 10, 2002

Machine-extracted title · confidence 95%

Daily instrument performance verification log for ICPMS analysis including intensity and standard deviation data for multiple elements.

NYC-WTC_000040452–000040596

Folder label: “ICPMS 4/10/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE07484 Sample Date/Time: Wednesday, April 10,2002 10:26:45 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: d:\elandata\Method\NEWQ200.8.mth Dataset File: d:\elandata\Dataset\NEWQ\NEWQ\AE07484.431 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit r Be 9 10.000 10.000 0.000 0.00111 158.66 ug/L > Se-1 45 515229.029 1.728 515229.029 ug/L Cr 52 11042.481 1.722 0.008 0.41984 0.25 ug/L Cr 53 1166.087 4.239 0.001 0.32659 18.55 ug/L Mn 55 273137.683 0.773 0.525 17.83520 1.93 ug/L Ni 60 853.049 3.774 0.002 0.34850 3.50 ug/L Cu 63 5599.448 3.044 0.010 0.90721 3.98 ug/L Cu 65 2636.409 2.399 0.005 0.95535 2.58 ug/L Zn 66 1325.110 2.001 0.005 0.29265 3.33 ug/L Zn 67 416.347 4.901 0.003 0.81730 6.63 ug/L Zn 68 1634.497 3.732 0.010 0.80221 4.37 ug/L Ge 72 99360.440 1.520 99360.440 ug/L As 75 1251.487 5.263 0.009 0.46841 5.04 ug/L Se 77 164.336 5.488 0.000 0.16157 26.49 ug/L Se 82 273.674 4.075 0.001 0.32088 20.93 ug/L Ag 107 1920.222 5.592 0.001 0.09884 12.09 ug/L In 115 1383700.315 1.406 1383700.315 ug/L Sb 121 1052.072 9.691 0.001 0.10769 11.50 ug/L Sb 123 807.566 9.051 0.001 0.10674 10.82 ug/L Ba 135 42922.862 1.153 0.023 15.21897 0.79 ug/L Ba 137 74899.043 1.006 0.040 15.23839 1.03 ug/L Ho 165 1874944.030 0.423 0.136 ug/L > Tb 159 1884027.516 1.009 1884027.516 ug/L TI 205 736.371 4.598 -0.000 -0.00464 25.81 ug/L Pb 208 3336.935 11.039 0.001 0.03809 29.57 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ' Be 9 > Sc-1 45 91.586 Cr 52 Cr 53 Mn 55 Ni 60 Cu 63

Sample ID: AE07484 Report Date/Time: Wednesday, April 10,2002 10:28:20 Page 1

NYC-WTC_000040477

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NYC-WTC_000040477Source: NYC Law Department, mirrored locally

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