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ICPMS daily performance check report, April 10, 2002

Machine-extracted title · confidence 95%

Daily instrument performance verification log for ICPMS analysis including intensity and standard deviation data for multiple elements.

NYC-WTC_000040452–000040596

Folder label: “ICPMS 4/10/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: LRB Sample Date/Time: Wednesday, April 10, 2002 10:05:49 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: d:\elandata\Method\NEWQ200.8.mth Dataset File: d:\elandata\Dataset\NEWQ\NEWQ\LRB.427 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit r Be 9 10.667 5.413 0.000 0.00219 55.94 ug/L > Se-1 45 523423.105 0.496 523423.105 ug/L Cr 52 7167.897 1.739 -0.000 -0.00171 784.86 ug/L Cr 53 545.689 5.773 -0.001 -0.23800 12.68 ug/L Mn 55 1713.846 4.050 -0.002 -0.06592 6.04 ug/L Ni 60 34.667 13.632 0.000 0.00293 66.10 ug/L Cu 63 229.339 4.052 -0.001 -0.07866 1.92 ug/L Cu 65 131.002 9.255 0.000 0.01336 34.36 ug/L Zn 66 704.368 0.499 -0.001 -0.06903 9.28 ug/L Zn 67 147.003 9.524 -0.000 -0.06831 62.43 ug/L Zn 68 546.355 8.034 -0.001 -0.05840 67.97 ug/L Ge 72 99540.358 1.139 99540.358 ug/L As 75 278.974 20.597 -0.000 -0.02035 134.41 ug/L Se 77 116.335 11.219 -0.000 -0.12679 58.13 ug/L Se 82 198.671 5.092 -0.000 -0.01508 236.37 ug/L Ag 107 1007.399 7.868 0.000 0.01699 38.15 ug/L > In 115 1387140.876 1.802 1387140.876 ug/L Sb 121 314.342 6.460 0.000 0.02874 7.11 ug/L Sb 123 260.237 20.105 0.000 0.03135 23.46 ug/L Ba 135 55.001 8.332 -0.000 -0.00060 281.97 ug/L Ba 137 91.335 8.290 0.000 0.00167 92.69 ug/L Ho 165 1888226.624 0.695 0.138 ug/L Tb 159 1892067.189 0.689 1892067.189 ug/L T1 205 732.037 6.460 -0.000 -0.00492 38.92 ug/L Pb 208 1747.082 1.630 -0.000 -0.00742 15.47 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ' Be 9 > Se-1 45 93.042 Cr 52 Cr 53 Mn 55 Ni 60 Cu 63

Sample ID: LRB Report Date/Time: Wednesday, April 10, 2002 10:08:23 Page 1

NYC-WTC_000040469

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NYC-WTC_000040469Source: NYC Law Department, mirrored locally

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