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GCMS reanalysis comments for sample AE03383, April 2002

Machine-extracted title · confidence 100%

Laboratory notes indicating high recoveries and the decision to reextract and reanalyze sample AE03383 on April 16, 2002.

NYC-WTC_000040156–000040163

Folder label: “GCMS X 3/26/02 A 4/6/02

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Scanned page image, NYC-WTC_000040160
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\APR0405\3383.D Vial: 19 • Acq On 6 Apr 2002 11:39 am Operator: Sample gc/ms scan 3/26 fb Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.249 779 785 801 rBV 896942 2332296 69.16% 15.764% 2 14.847 1063 1068 1072 rBV2 52045 102003 3.02% 0.689% 3 15.884 1175 1181 1199 rBV 1391152 2989389 88.65% 20.205% 4 21.190 1752 1759 1767 rBV 1584823 3372107 100.00% 22.792% 5 23.329 1986 1992 1998 rVB 92364 182660 5.42% 1.235%

6 25.634 2236 2243 2253 rBV 1434624 3109645 92.22% 21.018% 7 33.685 3112 3120 3136 rBV2 727532 1678037 49.76% 11.342% 8 37.926 3575 3582 3597 rBV2 345481 1028962 30.51% 6.955%

Sum of corrected areas: 14795099

3383.D GCMS0408.M Mon Apr 15 14:43:26 2002

NYC-WTC_000040160

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NYC-WTC_000040160Source: NYC Law Department, mirrored locally

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