GCMS reference data for sample AE06585, April 15, 2002

!UCit-wU-LL RUpUA \+ IC V C wUU/

2 2 - X p Data File : C:\MSDCHEM\l\DATA\041502\REFA0415.D Acq On Vial: 6 O co : 15 Apr 2002 2:08 pm Operator: Bohlk __ s Sample : REFI 3/20/02 Inst : Instrumen O Mise Multiplr: 1.00 "O 1 C o MS Integration Params: BENZO.P O o o o Quant Time: Apr 17 16:38 2002 Quant Results File: 5080402BBC.RES o C "0 CO o 00 Method : C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator) — 9 Title : Quantitation For Method 508gcscan Last Update : Tue Apr 16 18:27:45 2002 o o Response via : Initial Calibration O C Abundance TIC: REFA0415.D 3 Q 2600000 —

2400000 00

3 o o 5 13 5O y 0) CM

2200000 E $ 5 I Z 8 t1 £ 8 §2 5 6 2000000 $ £

li 1800000 11

$ 1600000 $ CI O t CM 2 79 1400000 8 £ 5( 8 6 1) s. 2 8 0) 3 s 5 a( 9 n.$ 5 D

i I S g. € tgs Q ra 2 1200000 O . - I- 2 3 0)

Is “5 t £ 6 il 8 3 I 15 X D

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1000000- Eg Gs G g 1f 5 “

H 3 —a g L •3 ac O 5 8 «9 8 3 II S || d £ S. 1 £ $ li 2 800000 d 9 88 1555 5 5#§58 8 § 84 S l $4 tn “ 0) 8 s8 f

4ta 2i n 11 O iff 8 0)

ij 8 5g or 6 5 § ls Q 600000 2 $8 CM 5 Q

43 II f 8 8 © H 2

400000 8E S. Na 08 6 s O 3 § cl m c

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200000 v I E f F • N —E Z X N p U z

0"— 'I 1 —- , M U. 111 - — i. — —.A An- Time—> 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36’00 38’00

REFA0415.D 5080402BBC.M Wed Apr 17 16:39:21 2002 Page 3