GCMS blank analysis for sample AE06760, April 16-19, 2002

Data File : C:\MSDCHEM\l\DATA\041602\REFA0416.D Vial: 5 Acq On : 16 Apr 2002 11:54 am Operator: Bohik Sample : REFI 3/21/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Apr 18 14:31 2002 Quant Results File: 5080402BBC.RES

Method : C:\MSDCHEM\1\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Tue Apr 16 18:27:45 2002 Response via : Initial Calibration Abundance TIC: REFA0416.D 2600000

% 2400000 o o 8 o y0 G g o 5 2200000 § £ s§ N

2 ci 5 CD 5 8 £ & 2000000 o § 1800000

1600000 $ o 5 £ § CD

g 1400000 5 8 2 5 2 s 0 3 5ro g I CM

8 9 D J2 a s §g 1 6 I € 1200000 fa 8s. d 0 3 - O 8 o 8 i s 11 £ S§ ss c Ms f @ o & o- £ s5 9 en 1000000 8 o.E 68 o o E. 88 CD 5 (d € g It 1526 S g to £ 2 8 m

5 gf i £ 800000 R in- £ 88 C 91 St 8a 11 f2 51 CD w -aNe 5 b 2 §8 8 O

C O 600000 2 8885 5 «S® 95 oo 3 18 0 5 $ CM CD 5 2 X e 9 § ii s 2 f 3 E $158 825 1 18 8 □ 8 O o Q 400000 g E 82 Q"3888 ■? « ole a x & 9 I 3 N 5 m 13 co t 8 F Z 8 8 6 N I" C O O O. o CL 200000 I 2 9 0 O) co X o

U O o o CL 0- ■ । ■ — — W (N lS Ir I TT r I । 1 1d o o I Time—> 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00 o o REFA0416.D 5080402BBC.M Thu Apr 18 15:46:48 2002 Page 3 5 u O > > 2 2