GCMS analysis results for sample AE06454, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE06454 conducted on April 19, 2002, by the DEP.

NYC-WTC_000039574–000039587

Folder label: “GCMS X 3/19/02 A 4/17/02”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

* Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR1702\6454.D Vial: 12 Acq On : 17 Apr 2002 6:59 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 6 3-Trimethylsilyloxystearic aci Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 37.31 0.58 ug/1 40595 Perylene-dl2 37.87

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Trimethylsilyloxystearic acid, tr 444 C24H5203Si2 000000-00-0 22 2 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 16 3 Benzophenone-2,45-tricarboxylic a 356 C19H1607 000000-00-0 10 4 Hexahydropyridine,/ 1-methyl-4-(4-hy 221 C13H19NO2 000000-00-0 9 Abundance Scan 3514 (37.307 min): 6454.D (-) Im/z 73.00 100.00% 73 147

5000 221 NNWW 1 281 355 AY WAA 429 I I I [ I I I [ [ I I I I I T I I I [ ( I I I [ 327

mz-> 44 Il I " l1' " i " "I' 46 i""l‘ TTT L 253 _ I 193 , |, r ri11 ■ ■ i ■" 11 1 ■1 ■ i "'' I 40 60 80 100120140160180200220240260280300320340360380400420 37.00 37.20 37.40 37.60 m/z 147.00 67.74% Abundance #56734: 3-Trimethylsilyloxystearic acid, trimethylsilyl est 73 //

5000 147 233 A_ ' 1 ' 1 1 ' 1 1 I 1 ' 1 > I ' ' 1 I I 37.00 37.20 37.40 37.60 11 I

313 429 m/z 221.05 50.16% 189 1, 339 TI—B1I10TCE—0I-TE1T " i" " r ‘" i'"' i" " ।।" r ■ ।. < A11*. >. p >.. ।।। TTTT * 111A । ] 387 1 mz—> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7- „PL ( 147 221 A....... _ 37.00 37.20 37.40 37.60 -.......... 73 5000 m/z 281.00 36.22%

117 191

H '1" i11111 1,. i11111'1111" " r1H lm' i11 “ I I 111 TTT 279 AAmu/ rn/z—> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #49884: Benzophenone-2,4', 5-tricarboxylic acid, trimethyl e 221 37.00 37.20 37.40 37.60 163 m/z 355.05 33.00%

5000

m/z—> mm T 76 103 135 325

111111111111" 1111'1111 ■1111111111111ri 111 40 60 80 100120140160180200220240260280300320340360380400420 356

V "I 1 1 1 1 | * 1 1 । | 1 1 1 ’ | zM IBE I I TT I I 1 I 1 I I IT 37.00 37.20 37.40 37.60 11 1 I 1 1 1 1 I A...

6454.D GCMS0412.M Thu Apr 18 09:13:23 2002 Page 6

NYC-WTC_000039586

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000039586Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

GCMS analysis results for sample AE06453, April 2002 · Box DEP Box 23

NYC-WTC_000039560

Laboratory report documenting GCMS analysis of sample AE06453 conducted on April 19, 2002, by the DEP.

1 shared topics · Same agency, volume and box · similarity 0.998