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GCMS analysis results for sample AE06449, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.

NYC-WTC_000039497–000039521

Folder label: “GCMS X 3/19/02 A 4/17/02

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Scanned page image, NYC-WTC_000039521
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NYC 9/11 Public Portal Document

Tentatively Identified Compound (LSC) summary

Operator ID: Date Acquired: 17 Apr 2002 2:06 pm Data File: C:\HPCHEM\1\DATA\APR1702\6449.D Name: gc/ms scan 3/19 Mise: Method: C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title: 209 625/TCLP calibration table Library Searched: C:\DATABASE\NBS75K.L

TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc

Silane, tetramethyl- 8.10 2.9 ug/1 382656 ISTD01 12.21 2598540 20.0 / Cyclotetrasiloxane , 11.61 0.4 ug/1 46204 ISTD01 12.21 2598540 20.0 ! Cyclopentasiloxane, 14.81 1.3 ug/1 210324 ISTD02 15.84 3269450 20.0 > Cyclohexasiloxane, d 17.97 2.0 ug/1 326690 ISTD02 15.84 3269450 20.0 ’ Imidazole-4-carboxam 18.68 0.8 ug/1 148897 ISTD03 21.15 3697390 20.0 ‘ Pentasiloxane, dodec 20.80 1.4 ug/1 258160 ISTD03 21.15 3697390 20.0 Benzoic acid,, 4-etho 21.56 0.4 ug/1 79774 ISTD03 21.15 3697390 20.0 Sil ane, 114-1,2-bi s 23.33 1.2 ug/1 219818 ISTD03 21.15 3697390 20.0 3 -Isopropoxy-1,1,1,7 25.49 1.0 ug/1 163815 ISTD04 25.58 3445620 20.0 1,1,1,5,7,7, 7-Heptam 27.43 0.6 ug/1 111787 ISTD04 25.58 3445620 20.0 Noradrenaline, tetra 29.19 0.5 ug/1 84439 ISTD04 25.58 3445620 20.0 3 -Isopropoxy-1,1,1,7 30.78 0.7 ug/1 77444 ISTD05 33.65 2264060 20.0 1,1,1,5, 7,7,7-Heptam 32.24 0.7 ug/1 74021 ISTD05 33.65 2264060 20.0 3-Trimet/hyl silyl oxys 34.89 0.5 ug/1 59877 ISTD05 33.65 2264060 20.0 Trisiloxcane, 1,1,1,5 36.09 0.9 ug/1 66783 ISTD06 37.87 1549720 20.0 3,6 -Dioxa-2,4,5,7-te 37.32 0.9 ug/1 67619 ISTD06 37.87 1549720 20.0 3,6-Dioxa-2,4,5,7-te 38.75 0.7 ug/1 54143 ISTD06 37.87 1549720 20.0 / 6449.D GCMS0412.M Thu Apr 18 09:11:00 2002

NYC-WTC_000039521

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NYC-WTC_000039521Source: NYC Law Department, mirrored locally

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