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GCMS analysis results for sample AE06430, April 2002

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Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.

NYC-WTC_000039469–000039496

Folder label: “GCMS X 3/19/02 A 4/17/02

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NYC 9/11 Public Portal Document

Tentatively Identified Compound (LSC) summary 6 Operator ID: Date Acquired: 17 Apr 2002 1:08 pm Data File: C:\HPCHEM\1\DATA\APR1702\6430.D Name: gc/ms scan 3/19 fb Mise: Method: C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title: 209 625/TCLP calibration table Library Searched: C:\DATABASE\NBS75K.L

TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc

Cyclotrisiloxane, he 7.59 0.3 ug/1 39082 ISTD01 12.21 2518470 20.0 Silane, tetramethyl- 8.10 4.0 ug/1 506816 ISTD01 12.21 2518470 20.0 Ethane, 1,1,2,2-tdtr 9.95 0.3 ug/1 39226 ISTD01 12.21 2518470 20.0 Cyclotetrasiloxane, 11.62 0.4 ug/1 52921 ISTD01 12.21 2518470 20.0 Cyclopentasiloxane, 14.81 1.5 ug/1 235059 ISTD02 15.85 3226510 20.0 Cyclohexasiloxane, d 17.97 3.1 ug/1 503633 ISTD02 15.85 3226510 20.0 Imidazole-4-carboxam 18.68 0.7 ug/1 133625 ISTD03 21.14 3584520 20.0 1,1,1,3,5,7,9,9, 9-No 20.80 2.3 ug/1 417541 ISTD03 21.14 3584520 20.0 Benzoic acid, A-etho 21.56 0.7 ug/1 131476 ISTD03 21.14 3584520 20.0 Phenethylamine, N-me 23.32 1.7 ug/1 298993 ISTD03 21.14 3584520 20.0 3-1sopropoxy/1,1,1,7 25.50 1.4 ug/1 232537 ISTD04 25.59 3314710 20.0 Trisiloxane, 27.42 1.0 ug/1 160353 ISTD04 25.59 3314710 20.0 oic aci ,2,6-bi 29.19 0.8 ug/1 129886 ISTD04 25.59 3314710 20.0 1,1,1,5, , 7,7 Hept 30.78 1.1 ug/1 127269 ISTD05 33.64 2332650 20.0 3-1sopropoxy-1,1,1,7 32.24 1.0 ug/1 111833 ISTD05 33.64 2332650 20.0 1,1,1,5,7 ,h,7-Heptam 34.90 0.8 ug/1 92473 ISTD05 33.64 2332650 20.0 Trisiloxane, 1,1,1,5 36.09 1.0 ug/1 80534 ISTD06 37.87 1640930 20.0 1,1,1,5,7, 7,7-Heptam 37.31 1.0 ug/1 84299 ISTD06 37.87 1640930 20.0 3,6-Dioxa-2,4,5,7-te 38.74 0.7 ug/1 57055 ISTD06 37.87 1640930 20.0 Trisiloxane, 1,1,1,5 40.49 0.5 ug/1 41749 ISTD06 37.87 1640930 20.0

6430.D GCMS0412.M Thu Apr 18 09:09:36 2002 (pRN

NYC-WTC_000039496

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NYC-WTC_000039496Source: NYC Law Department, mirrored locally

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