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GCMS raw data printout for sample AE05913, March 2002

Machine-extracted title · confidence 100%

Raw GCMS data file printout showing chromatographic peaks and retention times for sample AE05913 analyzed on March 18, 2002.

NYC-WTC_000039162–000039167

Folder label: “GCMS X 3/14/02 A 3/17/02

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NYC 9/11 Public Portal Document

/ Quantitation Report (QT Reviewed)

.Data File : C:\MSDCHEM\l\DATA\031702\5908.D Vial: 27 Acq On : 18 Mar 2002 7:40 am Operator: McLean Sample : 3/14/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Mar 20 11:04:24 2002 Quant Results File: 5080302.RES

Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Thu Mar 14 13:02:27 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.54 150 1300456 20.00 ug/L 0.00 10) Naphthalene-d8 13.03 136 3603717 20.00 ug/L 0.00 17) Acenaphthene-diO 18.13 164 1993336 20.00 ug/L 0.00 29) Phenanthrene-dlO 22.50 188 3035318 20.00 ug/L 0.00 38) Chrysene-dl2 30.30 240 2865965 20.00 ug/L -0.02 44) Perylene-dl2 34.18 264 1729898 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-ddd surr 27.43 235 269758 7.45 ug/L 0.00 Spiked Amount 5.000 Recovery = 149.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. d 3) bis(2-chloroethyl) ether 0.00 93 0 N.D. 4) 1,3 - Dichlorobenze 0.00 146 0 N.D. 5) 1,4 - Dichlorobenzene 0.00 146 0 N.D. 6) 1,2 - Dichlorobenzene 0.00 146 0 N.D. 7) 2,2 1 - oxybis (l-Chloropr 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy) methan 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenyl ethe 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 30) N-Nitrosodiphenylamine 0.00 169 0 N.D. 31) 4-Bromophenyl-phenyl ether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 0.00 178 0 N.D. d 34) Anthracene 22.69 178 10390 0.07 ug/L 97 35) Di-n-butylphthalate 24.65 149 37636 0.23 ug/L 89 36) Fluoranthene 0.00 202 0 N.D. d 39) Pyrene 0.00 202 0 N.D. d 40) Butylbenzylphthalate 29.05 149 13470 0.16 ug/L 85 41) Benzo (a) antracene 30.28 228 181612 1.21 ug/L 97 42) Bis (2-ethylhexyl) phthala 30.91 149 111789 1.00 ug/L 99 43) Chrysene 30.37 228 314739 2.20 ug/L 98 45) Di-n-Octylphthalate 32.75 149 133083m 0.72 ug/L 46) Benzo (b) fluoranthene 33.23 252 121457 1.00 ug/L 98

(#) = qualifier out of range (m) = manual integration 5908.D 5080302.M Wed Mar 20 11:41:53 2002 Page 1

NYC-WTC_000039162

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