Laboratory report documenting GCMS analysis of sample AE02095 conducted on March 20, 2002, showing surrogate compound data.
NYC-WTC_000038958–000038965Folder label: “GCMS X 3/8/02 A 3/19/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed) • W Data File : C:\MSDCHEM\1\DATA\031802\2095.D Vial: 22 Acq On : 19 Mar 2002 7:21 pm Operator: McLean Sample : GC/MS SCAN 3/8 FB Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Mar 20 06:48:38 2002 Quant Results File: 5080302.RES
Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Thu Mar 14 13:02:27 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 9.54 150 1321104 20.00 ug/L 0.00 10) Naphthalene-d8 13.03 136 3698404 20.00 ug/L 0.00 17) Acenaphthene-diO 18.13 164 2055350 20.00 ug/L 0.00 29) Phenanthrene-diO 22.50 188 3100338 20.00 ug/L 0.00 38) Chrysene-dl2 3 0.30 240 2858406 20.00 ug/L -0.02 44) Perylene-dl2 34.18 264 1524794 20.00 ug/L 0.00
System Monitoring Compounds 37) 2,4-ddd surr 27.43 235 207446 5.61 ug/L 0.00 Spiked Amount 5.000 Recovery = 112.20%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-chloroethyl) ether 0.00 93 0 N.D. 4) 1,3 - Dichlorobenze 0.00 146 0 N.D. 5) 1,4 - Dichlorobenzene 0.00 146 0 N.D. 6) 1,2 - Dichlorobenzene 0.00 146 0 N.D. 7) 2,2 ' - oxybis (l-Chloropr 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Is ophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy) methan 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 0.00 14 9 0 N.D. 26) 4-Chlorophenyl-phenyl ethe c. 00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 30) N-Nitrosodiphenylamine 0.00 169 0 N.D. 31) 4-Bromophenyl-phenyl ether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 0.00 178 0 N.D. 34) Anthracene 0.00 178 0 N.D. 35) Di-n-butylphthalate 0.00 149 0 N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 14 9 0 N.D. 41) Benzo (a) antracene 0.00 228 0 N.D. d 42) Bis (2-ethylhexyl) phthala 0.00 149 0 N.D. 43) Chrysene 0.00 228 0 N.D. d 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo (b) fluoranthene 0.00 252 0 N.D.
(#) = qualifier out of range (m) = manual integration 2095.D 5080302.M Wed Mar 20 06:49:44 2002 Page 1
NYC-WTC_000038960
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