NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
• Data File : C:\MSDCHEM\l\DATA\031802\2145.D Vial: 23
Acq On : 19 Mar 2002 8:10 pm Operator: McLean
Sample : GC/MS SCAN 3/8 Inst Instrumen
Mise : Multiplr: 1.00
MS Integration Params: BENZO.P
Quant Time: Mar 20 02:18:30 2002 1Quant Results File: 5080302.RES
Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator)
Title : Quantitation For Method 508gcscan
Last Update : Thu Mar 14 13:02:27 2002
Response via : Initial Calibration
DataAcq Meth : 508SCAN
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 9.54 150 1202962 20.00 ug/L 0.0 0
10) Naphthalene-d8 13.02 136 3324035 20.00 ug/L 0.00
17) Acenaphthene-dl0 18.13 164 1866080 20.00 ug/L 0.00
29) Phenanthrene-diO 22.50 188 2802531 20.00 ug/L 0.00
38) Chrysene-dl2 3 0.30 240 2493812 20.00 ug/L -0.02
44) Perylene-dl2 34.18 264 1322295 20.00 ug/L 0.00
System Monitoring Compounds
37) 2,4-ddd surr 27.43 235 199380 5.96 ug/L 0.00
Spiked Amount 5.000 Recovery = 119.20%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 3.24 74 5317 0.20 ug/L 100
3) bis(2-chloroethyl) ether 0.00 93 0 N.D.
4) 1,3 - Dichlorobenze 0.00 146 0 N.D.
5) 1,4 - Dichlorobenzene 0.00 146 0 N.D.
6) 1,2 - Dichlorobenzene 0.00 146 0 N.D.
7) 2,2 ' - oxybis (l-Chloropr 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) Isophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy) methan 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 0.00 128 0 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 18.13 165 236381 10.92 ug/L # 25 X
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 0.00 149 0 N.D.
26) 4-Chlorophenyl-phenyl ethe 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
30) N-Nitrosodiphenylamine 0.00 169 0 N.D.
31) 4-Bromophenyl-phenyl ether 0.00 248 0 N.D.
32) Hexachlorobenzene 0.00 284 0 N.D.
3 3) Phenanthrene 0.00 178 0 N.D. d
34) Anthracene 0.00 178 0 N.D. d
35) Di-n-butylphthalate 24.65 149 6465 0.04 ug/L 79
36) Fluoranthene 0.00 202 0 N.D.
3 9) Pyrene 0.00 202 0 N.D.
40) Butylbenzylphthalate 0.00 149 0 N.D.
41) Benzo (a) antracene 0.00 228 0 N.D. d
42) Bis (2-ethylhexyl) phthala 30.91 149 17697 0.18 ug/L 83
43) Chrysene 0.00 228 0 N.D. d
45) Di-n-Octylphthalate 0.00 149 0 N.D.
46) Benzo (b) fluoranthene 0.0 0 252 0 N.D.
(#) = qualifier out of range (m) = manual integration
2145.D 5080302.M Wed Mar 20 02:19:13 2002 Page 1
NYC-WTC_000038968
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