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GCMS calibration results for sample AE02092, March 2002

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Laboratory form detailing analytical methods and parameters including drip rate and pH for a sample analyzed on March 19, 2002.

NYC-WTC_000038914–000038917

Folder label: “GCMS X 3/8/02 A 3/19/02

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NYC 9/11 Public Portal Document

User: Fakhouri, Morgan Westchester Dept, of Labs & Research Date: 03/19/2002 Time: 15:39:42

Sample: AE02092 Analysis: SC1GCMS CALI GCMS Units: ug Started: 3/19/02 14:54 Ended: 3/19/02 14:54 Analyst: MF Page: 1

-Component Name Viol Result Qualifier MDL " 1:' n-Nitrosodimethylamine 39.65 2.0 ' 2 bis(2-Chloroethyl)ether 37.55 2.0 3 1,3-Dichlorobenzene 37.55 2.0 4 1,4-Dichiorobenzene 37.60 2.0 5 1,2-Dichlorobenzene 37.01 2.0 6 " 2,2'-oxybis(1 -Chloropropane) 7 39.25 2.0 ' 2.0 n-Nitrosodi-n-propylamine 40.09 8 Hexa chloroethane 37.88 ' 2.0 9 Nitrobenzene 38.34 2.0 ! 10 Isophorone 38.85 2.0 111 112. bis(2-Chioroethoxy)methane 37.90 2.0 '2.0 113 1,2,4-Trichlorobenzene 37.88 Naphthalene 37.44 2.0 14 Hexa chlorobutadiene 38.64 2.0 15 2-Chloronaphthalene 38.26 2.0 -17 16 Dimethylphthalate 39.31 2.0 18 2,6-Dinitrotoluene 39.75 2.0 Acenaphthylene 38.35 2.0 19 Acenaphthene 38.07 2.0 20 2,4-Dinitrotoluene 40.64 2.0 21 Diethylphthalate 38.54 2.0 22 4-Chlorophenylphenylether 38.38 2.0 23 Fluorene 37.33 2.0 24 Azobenzene/1,2-Diphenylhydraz 40.89 2.0 25 n-Nitrosodiphenylamine 37.95 2.0 26 4-Bromophenylphenylether 37.37 2.0 27 Hexa chlorobenzene 37.60 2.0 28 Phenanthrene 37.34 2.0 29 Anthracene 36.81 2.0 30 Di-n-butylphthalate 38.61 2.0 31 Fluoranthene 38.52 2.0 32 Pyrene 36.12 2.0 _ 33 Butyibenzylphthalate 37.23 2.0 34 Benzo(a)anthracene 38.44 2.0 35 . bis(2-Ethylhexyl)phthaIate 35.60 2.0 36 Chrysene 37.96 2.0 ,37 Di-n-octylphthalate 37.35 2.0 38 Benzo(b)fluoranthene 39.57 2.0 ‘“39 Benzo(k)fluoranthene 39.65 2.0 40, Benzo(a)pyrene 39.09 2.0 41. Indeno(1,2,3-cd)pyrene 40.60 2.0 42: Dibenz(a,h)anthracene 41.14 2.0 43 | Benzo(g,h,i)perylene 41.38 2.0

NYC-WTC_000038914

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