Gas chromatography-mass spectrometry analysis of environmental samples for polycyclic aromatic hydrocarbons including naphthalene, phenanthrene, chrysene, and perylene.
NYC-WTC_000038465–000038472Folder label: “GCMS X 2/26/02 A 2/28/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File C:\MSDCHEM\l\DATA\022802\01335 .D Vial: 23 Acq On 1 Mar 2002 6:36 am Operator: McLean Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Mar 13 06:43:13 2002 Quant Results File: 5080202.RES
Quant Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Mon Feb 25 19:17:14 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) l,4-Dichlorobenzene-d4 9.58 15C 1129522 20.00 ug/L 0.00 10) Naphthalene-d£ 13.05 136 2965041 20.00 ug/L 0.00 17) Acenaphthene-diO 18.16 164 1652257 20.00 ug/L 0.00 29) Phenanthrene-diO 22.52 188 2558209 20.00 ug/L 0.00 38) Chrysene-dl2 30.33 240 2358694 20.00 ug/L -0.03 44) Perylene-dl2 34.21 264 1479035 20.00 ug/L -0.02
System Monitoring Compounds 37) 2,4-ddd surr 27.46 235 216796 5.34 ug/L 0.00 Spiked Amount 5.000 Recovery = 106.80%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. d 3) bis(2-chloroethyl) ether 0.00 93 0 N.D. 4) 1,3 - Dichlorobenze 0.00 146 0 N.D. 5) 1,4 - Dichlorobenzene 0.00 146 0 N.D. 6) 1,2 - Dichlorobenzene 0.00 146 0 N.D. 7) 2,2 1 - oxybis (l-Chloropr 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy) methan 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 18.16 165 210488 9.16 ug/L # 25 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenyl ethe 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 30) N-Nitrosodiphenylamine 0.00 169 0 N.D. 31) 4-Bromophenyl-phenyl ether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 0.00 178 0 N.D. 34) Anthracene 0.00 178 0 N.D. 35) Di-n-butylphthalate 0.00 149 0 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 4 0) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo (a) antracene 0.00 228 0 N.D. d 42) Bis (2-ethylhexyl) phthala 30.94 149 88463 0.83 ug/L 96 43) Chrysene 0.00 228 0 N.D. d 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo (b) fluoranthene 0.00 252 0 N.D.
(#) = qualifier out of range (m) = manual integration 01335.D 5080202.M Wed Mar 13 09:09:24 2002 Page 1
NYC-WTC_000038465
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NYC-WTC_000038431
Quantitation report listing response data for deuterated internal standards and surrogates from a March 14, 2002 analysis.
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Quantitation report listing response data for deuterated internal standards and surrogates from a March 14, 2002 analysis.
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Quantitation report listing response data for deuterated internal standards and surrogates from a March 14, 2002 analysis.
1 shared topics · Same agency, volume and box · similarity 0.987
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Raw data file printout from GCMS analysis of sample AE05903 showing chromatographic peaks and retention times.
1 shared topics · Same agency, volume and box · similarity 0.986
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Raw data file printout from GCMS analysis of sample AE05902 showing chromatographic peaks and retention times.
1 shared topics · Same agency, volume and box · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039076
Raw GCMS data file printout showing chromatographic peaks and retention times for sample AE05904 analyzed on March 18, 2002.
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Raw GCMS data file printout showing chromatographic peaks and retention times for sample AE05913 analyzed on March 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038391
Laboratory report listing quantitative results for various organic compounds in sample AE03454 from March 13, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038730
Laboratory data recording surrogate recovery and unknown compound screening for sample AE04511 dated April 4, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052477
Instrument data file from February 2002 listing retention times and concentrations for polycyclic aromatic hydrocarbon surrogates.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003911
Laboratory report for sample AE01910 showing GCMS analysis of unknown compounds and surrogate recovery on March 7, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052471
Instrument data file from February 2002 listing retention times and concentrations for polycyclic aromatic hydrocarbon surrogates.
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