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GCMS quantitation results for sample AE03454, March 2002

Machine-extracted title · confidence 95%

Quantitation report listing response data for deuterated internal standards and surrogates from a March 14, 2002 analysis.

NYC-WTC_000038405–000038413

Folder label: “GCMS X 2/26/02 A 2/28/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File C:\MSDCHEM\l\DATA\022802\03454FB.D Vial: 29 • Acq On 1 Mar 2002 11:32 am Operator: McLean Sample MS CSAN FB Q Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R. T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total" 1 9.579 712 717 738 rBV 2026121 5026022 69.01% 12.474% 2 12.083 988 993 997 rBV 376229 614803 8.44% 1.526% 3 13.053 1095 1100 1113 rBV 3620135 6781881 93.11% 16.832% 4 18.160 1657 1663 1677 rBV 3659006 7283455 100.00% 18.077% 5 22.523 2138 2144 2158 rBV2 3452932 7242802 99.44% 17.976% 6 22.677 2158 2161 2170 rVB 26140 74081 1.02% 0.184% 7 27.457 2684 2688 2700 rVB 603474 1054093. 14.47% 2.616% 8 30.332 2998 3005 3025 rBV2 2983223 6827822 93.74% 16.947% 9 30.940 3067 3072 3080 rBV 82988 183083 2.51% 0.454% 10 34.214 3425 3433 3456 rBV2 2095166 5202377 71.43% 12.912%

Sum of corrected areas: 40290419

J454FB.D 5080202.M Wed Mar 13 06:53:23 2002 Page 1

NYC-WTC_000038410

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NYC-WTC_000038410Source: NYC Law Department, mirrored locally

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