GCMS internal standard quantitation results, Mar 13 2002

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2 2 K Data File C:\MSDCHEM\l\DATA\022802\REFB0226.D Vial: 18 o o 3o Acq On Sample Mise 1 Mar 2002 2:31 am Operator: McLean Inst : Instrumen Multiplr: 1.00 to _ s

1o MS Integration Params: BENZO.P "0 C o Quant Time: Mar 13 11:15 2002 Quant Results File: 5080202.RES O o C o o 00 "0 co Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator) o 00 Title : Quantitation For Method 508gcscan — CH 9 Last Update : Mon Feb 25 19:17:14 2002 U Response via : Initial Calibration o O Abundance TIC: REFB0226.D C 4500000 3 0 D

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I!i S. E 2000000 s8 S a f gB E I e r g 2 CD Il o o I §‘ t If I 1500000 i 1 § I 8 - i c o T a 8 O

s s ’ f 114 § £

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1000000 f $26 G oi 4 C o § 1 Js N 3 1 5 8 S 5 I I * A “2 e to

1 1 0 « 500000 I I X x X

Tlme-> 0 TITT i r I i i 4.00 6.00 Ju L U 8.00 10.00 — 12.00 u... — 18.00 — I, 14.00 20.00 22.00 ' 16.00 24.00 । —Ir i 26.00 fT IT 1 I ' 28.00 30.00 1 32.00 34.00 I r — T

36.00 38.00

REFB0226.D 50802.02.M Wed Mar 13 11:16:01 2002 Page 3