GCMS analysis results for sample AE04027, Mar 18 2002

NYC 9/11 Public Portal Document Library searen compound Keporc

Data File : C:\HPCHEM\1\DATA\FEB2102\4027.D Vial: 82 Acq On : 25 Feb 2002 2:41 am Operator: Sample : gc/ms scan 2/22 Inst : GC/MS 2 09 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,3-Dioxolane, 2-(3-bromo-5,5, Concentration Rank 1

R.T. EstConc . Area Relative to ISTD R.T.

8.20 3.78 ug/1 193126 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 17 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 Pentane, 3-methoxy­ 102 C6H140 036839-67-5 9 Abundance C Scan 344 (8.203 min): 4027.D (-) m/ z 73.00 100.00% i 73

5000 43 i 87 7.80 8.00 8.20 8.40 8.60 103 im/z--> t ' ■

10 ■ ' i ■

20 30 • ■ ■ i ' 70 lL — ----- 40 80 50 55 90 ir 100 ■ 110 ‘II 60 । 1

120 m/z 42.95 29.18% Abundance #49423: 1.3-Dioxolane. 2-(3-bromo-5,5.5-trichloro-2,2-dimet 73 .... ----------- 5000 7.80 8.00 8.20 8.40 8.60 45 m/Z 41.05 10.87% 36 , li 55 67, , ......... 109 115 i ■ ■ ■ • i ■ ■ ■ ■ i • • I • i ■ ‘ • FWr0nnnn11n/1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide 30 73 7.80 8.00 8.20 8.40 8.60 5000 m/ z 44.95 10.52% I • 58 I 44 i

15 I i ■ ■ ■ ■ i ■ ■ ■ ■ । ■ ■ ■ ■ । 1

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance . #845: Silane, tetramethyl- I 73 7.80 8.00 8.20 8.40 8.60 m/z " 6.80% 5000

45 1 1 ' ' 10 15 ■

20 i ■ ■ ■ ■ i'1

30 31 -155 40 50 ...... |..... 88................ 60 70 80 90 100 110 120 7.80 8.00 8.20 8.40 8.60

4027.D GCMS0208.M Wed Mar 13 11:41:37 2002 Page 1

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