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GCMS blank analysis results, sample AE03833, Mar 13 2002

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Laboratory report documenting GCMS blank analysis for sample AE03833 conducted on March 13, 2002.

NYC-WTC_000038265–000038272

Folder label: “GCMS X 2/22/02 A 2/24/02

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Scanned page image, NYC-WTC_000038271
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Data File : C:\HPCHEM\1\DATA\FEB2102\LBE.D Vial: 70 Acq On : 24 Feb 2002 2:55 pm Operator: Sample : gc/ms scan 2/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L

Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.20 4.48 ug/1 277865 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW Mol Form’ CAS# Qual

1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 3 1,3-Dioxolane, 2-pentadecyl- 284 C18H36O2 004360-57-0 9 4 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 7 Abundance I ' Scan 344 (8.198 min): LBE.D (-) m/z 73.00^100.00% 73

5000- 43 7.80 8.00 8.20 8.40 . 8.60 57 ■ i ■ ■ ■ ' I' ■ T 'i ■ ■ ■ 87 103 m/ z 42.95 28.59% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #292: N-Ethylformamide 30 73

5000- 44 58 7.80 8.00 20 8.40 8.60 m/ z 44.95 10.78% 15 ■ ■ । ■ > • ■ । ■ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 'Abundance #62932: Silane, tetramethyl- 73

7.80 8.00 8.20 8.40 3.60 5000 m/z 41.0.5 10.38% 45 15 j 59 88 , ..... 1 ' i ■ TTTTrT miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #40191: 1,3-Dioxolane, 2-pentadecyl- 73 7.80 8.00 8.20 8.40 8.60 m/z 71.00 6.64% 5000 -

— 57 ■ ■ i ■ • > • I............. । 86 99 256 283 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 7.80 8.00 8.20 8.40 8.60 |

LBE.D GCMS0208.M Wed Mar 13 11:42:13 2002 Page 1

NYC-WTC_000038271

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NYC-WTC_000038271Source: NYC Law Department, mirrored locally

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