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GCMS analysis results for sample AD31499, Feb 27 2002

Machine-extracted title · confidence 100%

Laboratory report listing detection results for volatile organic compounds in sample AD31499 analyzed on February 27, 2002.

NYC-WTC_000038139–000038148

Folder label: “GCMS X 2/21/02 A 2/22/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\31499.D Vial: 35 Acq On : 23 Feb 2002 12:39 am Operator: Sample : gc/ms scan 2/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.88 0.24 ug/1 25261 Phenanthrene-dl0 25.74

Hit# of 5 tentative/ ID • MW MolForm CAS# Qual

1 Phenanthrene-dlC 001517-22-2 91 188 C14D10 2 Anthracene-Al0- 001719-06-8 86 188 C14D10 3 Phosphonic acid. (3-methyl-3-penten 188 C8H13O3P1 022152-34-7 53 4 1,4-Naphthalenedione, 2-hydroxy-3-m 188 C11H803 000483-55-6 9 Abundance 7 Scan 2269 (25.875 min): 31499.D (-) m/z 188.10 100.00% 188

5000 ,.............. 66 80 92 158 25.60 25.80 26.00 26.20 ...... 44, ML — m/z 189.10 20.39% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188

_ 5000 I ' • 25.60 25.80 26.00 26.20 m/z 79.95 16.80% . 80 94 160 —..... ... ..... 1 i..................।।11............. । ll .. m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

1 25.60 25.80 26.00 26.20 i 5000 m/z 184.10 13.95%

80 94 160 66 ■ i ■ ■ ■' i ■ ■ ■111'' ■ i' ■'' i ■ । r, .y । >.. 1111TITETT 1111 rq-i ’ ’0’1’117111111111 miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19736: Phosphonic acid, (3-methyl-3-penten-1-ynyl)-. dimet — 188 25.60 25.80 26.00 26.20 m/z 66 . 05 13.29%

5000 77 62 35 47 93 109 155 _ ........ •......... ....... ........................ .................. / ' I' ■'' I • ‘ TTTTTT 11 T Tr 11" 11..........11111111111111111 ..11.■..।,11■<,,।, TTT T ..... "IT 11 ■ ■ i ' r ■ ■ I m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

31499.D GCMS0208.M Wed Feb 27 12:00:31 2002 Page 2

NYC-WTC_000038147

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NYC-WTC_000038147Source: NYC Law Department, mirrored locally

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