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GCMS analytical results for sample AE03825, March 29, 2002

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Laboratory report listing detection results for volatile organic compounds in sample AE03825 analyzed on March 29, 2002.

NYC-WTC_000038032–000038041

Folder label: “GCMS X 2/20/02 A 3/22/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) 9

Data File C:\HPCHEM\l\DATA\MAR2202\3825.D Vial 6 Acq On 22 Mar 2002 11:03 pm Operator Sample gc/ms scan 2/20 Inst GC/MS 209 Mise Multiplr 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 26 14:30 2002 Quant Results File: GCMS0308.RES

Quant Method C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title 209 625/TCLP calibration table Last Update Tue Mar 26 14:13:06 2002 Response via Initial Calibration DataAcq Meth GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.65 178 625 N.D. 34) Anthracene 25.72 178 205 N.D. 35) Di-n-butylphthalate 27.62 149 3700 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 32.14 149 1479 N.D. 41) Benzo(a)anthracene 33.79 22 8 182 0 N.D. 42) Bis(2-ethylhexyl)phthalate 33.93 149 26031 0.90 ug/1 95 43) Chrysene 33.79 228 1907 N.D. 45) Di-n-Octylphthalate 35.67 149 4096 N.D. 46) Benzo(b)fluoranthene 3.6.78 252 2322 N.D. 47) Benzo(k)fluoranthene 36.83 252 2478 N.D. 48) Benzo(a)pyrene 37.76 252 1867 N.D. 49) Indeno(1,2,3-cd)pyrene 42.12 276 783 N.D. 50) Dibenz(a,h)anthracene 42.23 278 583 N.D. 51) Benzo(g,h,i)perylene 43.36 276 1235 N.D.

(#) = qualifier out of range (m) = manual integration 3825.D GCMS0308.M Tue Mar 26 14:31:50 2002 Page 2

NYC-WTC_000038035

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NYC-WTC_000038035Source: NYC Law Department, mirrored locally

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