NYC-WTC_000012295
Laboratory report for GC/MS blank analysis of sample AE04417 conducted on March 22, 2002.
1 shared topics · similarity 0.996
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GCMS blank analysis results for sample AE03823, March 26, 2002
Machine-extracted title · confidence 100%Gas chromatography-mass spectrometry blank analysis for multiple chlorinated organic compounds with detection limits, completed March 26, 2002.
NYC-WTC_000038004–000038012Folder label: “GCMS X 2/20/02 A 3/22/02”
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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) 4 r V Data File : C:\HPCHEM\l\DATA\MAR2202\LB.D Vial 3 Acq On : 22 Mar 2002 8:06 pm Operator Sample :'gc/ms scan 2/20 Inst GC/MS 209 Mise : Multiplr 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 26 14:19 2002 Quant Results File: GCMS0308.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Mar 26 14:13:06 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.26 152 395323 20.00 ug/1 -0.09 10) Naphthalene-d8 15.90 136 1538318 20.00 ug/1 -0.09 17) Acenaphthene-diO 21.21 164 823831 20.00 ug/1 -0.10 29) Phenanthrene-diO 25.65 188 1227222 20.00 ug/1 -0.11 38) Chrysene-dl2 33.72 240 814067 20.00 ug/1 -0.12 44) Perylene-dl2 37.97 264 527331 20.00 ug/1 -0.15
System Monitoring Compounds 37) 2,4-DDD 30.73 235 85911 8.55 ug/mL 0.23 Spiked Amount 5.000 Recovery 17100* 4 30% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.0.0 74 0 N.D. 3) bis(2-Chloroethyl )ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 .0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.96 128 215 N.D. 16) Hexachlorobutadiene 0.00 22 5 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 . 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylph.thalate 22.68 149 324 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration LB.D GCMS0308.M Tue Mar 26 14:21:06 2002 Page 1
NYC-WTC_000038005
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NYC-WTC_000038005Source: NYC Law Department, mirrored locally
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