NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\MAR2502\LB.D Vial: 9
Acq On : 25 Mar 2002 6:05 pm Operator:
Sample : gc/ms scan 2/28 Inst : GC/MS 209
Mise : Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Mar 28 11:05 2002 Quant Results File: GCMS0308.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Tue Mar 26 14:13:06 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0308
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.25 152 539272 20.00 ug/1 -0.10
10) Naphthalene-d8 15.88 136 2071385 20.00 ug/1 -0.11
17) Acenaphthene-diO 21.19 164 1106205 20.00 ug/1 -0.12
29) Phenanthrene-diO 25.63 188 1586054 20.00 ug/1 -0.13
38) Chrysene-dl2 33.69 240 858147 20.00 ug/1 -0.15
44) Perylene-dl2 37.94 264 510240 20.00 ug/1 -0.18
System Monitoring Compounds
37) 2,4-DDD 30.71 235 108118 8.33-ug/mL 0.21
Spiked Amount 5.000 Recovery = —166. 60'% ff77a
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 0.00 74 0 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) 1sophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 15.26 93 196 N.D.
14) 1,2,4-Trichiorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.94 128 538 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
2 2) Acenaphthylene 0.00 152 0 N.D.
2 3) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 21.45 165 307 N.D.
25) Diethylphthalate 22.67 149 246 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 22.81 166 208 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
LB.D GCMS0308.M Thu Mar 28 11:06:28 2002 Page 1
NYC-WTC_000011838
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