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GCMS blank results for sample AE03799, March 22, 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of a method blank for sample AE03799 to verify analytical system cleanliness.

NYC-WTC_000037848–000037869

Folder label: “GCMS X 2/20/02 A 3/20/02

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Scanned page image, NYC-WTC_000037854
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

6 ' Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\031902\220LB.D Vial: 8 Acq On : 19 Mar 2002 5:24 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclotetrasiloxane, octamet... Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 8.91 0.68 ug/L 254484 . 1,4-Dichlorobenzene-d4 9.54

Hit# of 5 Tentative ID MW MolForm CAS# Qual --------------------------------------------------------------------- 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 91 2 Cyclotetrasiloxane, octamethyl- ... 296 C8H2404Si4 000556-67-2 91 3 Cyclotetrasiloxane, octamethyl- ... 296 C8H2404Si4 000556-67-2 90 4 Cyclotetrasiloxane, octamethyl- . 296 C8H24O4Si4 000556-67-2 72 undance Scan 643(8.908 min): 220LB.D (-) m/z 281.00 100.00 21

5000

133 193 249265 8.60 8.80 9.00 9.20 45 73 103 177 m/z 282.00 28.39 0 -> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 undance _44215: Cydotetrasiloxane, octamethyl- 21

5000 8.60 8.80 9.00 9.20 m/z 283.10 19.10 16117193 2492 25 51 73 103 133 ii 209 233 299 0 -> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 bundance #244218: Cyclotetrasiloxane, octamethyl- (CAS) $$1,1,3,3,... 21

8.60 8.80 9.00 9.20 5000 m/z 265.00 9.20

133 177193 221 249265 45 73 297 0 ritz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 undance #244216: Cyclotetrasiloxane, octamethyl- (CAS) $$ 1,1,3,3,... 21 8.60 8.80 9.00 9.20 m/z 193.00 9.09

5000

133 249265 0 28 45 73 103 177193209 -> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 8.60 8.80 9.00 9.20

220LB.D 5080302.M Thu Mar.21 11.52-'42 2nn2 Paae 3

NYC-WTC 000037854

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NYC-WTC_000037854Source: NYC Law Department, mirrored locally

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