Laboratory report documenting GCMS analysis of a method blank for sample AE00364 to verify analytical system cleanliness.
NYC-WTC_000037837–000037847Folder label: “GCMS X 2/20/02 A 3/20/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
S Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\FEB1102\364.D Vial: 18 Acq On : 12 Feb 2002 2:45 am Operator: 209 GALOS Sample : GC/MS SCAN 1/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 19 9:51 2002 Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.35 152 278324 20.00 ug/1 0.00 10) Naphthalene-d8 15.99 136 1067577 20.00 ug/1 -0.01 17) Acenaphthene-diO 21.30 164 569627 20.00 ug/1 -0.01 29) Phenanthrene-diO 25.75 188 841542 20.00 ug/1 -0.01 38) Chrysene-dl2 33.82 240 551375 20.00 ug/1 -0.02 44) Perylene-dl2 38.11 264 336170 20.00 ug/1 -0.01
System Monitoring Compounds 37) 2,4-DDD 30.83 235 51268 6.07 ug/mL 0.33 Spiked Amount 5.000 Recovery = 121.40%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. a
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 6) 1,2-Dichlorobenzene 7) 2,2'-oxybis(1-Chloropropan 8) N-Nitroso-di-n-propylamine 9) Hexachloroethane 11) Nitrobenzene 0.00 0.00 0.00 0.00 0.00 13.54 146 146 45 70 117 77 82 0 0 0 0 0 297 0 N.D. N.D. N.D. N.D. N.D. N.D. N.D. V, 12) 1sophorone 0.00 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 16.05 128 990 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Ac enapht hene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.77 149 478 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (nt) = manual integration 364.D GCMS0208.M Fri Mar 01 12:12:55 2002 Page 1
NYC-WTC_000037839
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NYC-WTC_000037927
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03801 conducted on March 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038974
Laboratory report documenting GCMS analysis of sample AE02146 conducted on March 21, 2002, showing surrogate compound data.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038966
Laboratory report documenting GCMS analysis of sample AE02145 conducted on March 20, 2002, showing surrogate compound data.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038958
Laboratory report documenting GCMS analysis of sample AE02095 conducted on March 20, 2002, showing surrogate compound data.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038941
Laboratory report documenting GCMS analysis of sample AE02093 conducted on March 20, 2002, showing surrogate compound data.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038933
Laboratory report documenting GCMS analysis of sample AE02092 conducted on March 20, 2002, showing surrogate compound data.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039237
Analytical data for sample AE08268 showing detection of unknown compounds and surrogate recovery on March 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039154
GCMS scan report for sample AE05913 listing results for unknown compounds analyzed on March 21, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012246
Laboratory report for GC/MS analysis of sample AE02087 conducted on March 25, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011177
Laboratory report documenting GC/MS analysis of environmental sample AE03182 conducted on March 22, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012207
Laboratory report for GC/MS analysis of sample AE02384 conducted on March 25, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011192
Laboratory report documenting GC/MS analysis of environmental sample AE03183 conducted on March 22, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000037819
Department of Environmental Protection site log sheet for the World Trade Center area covering February and March 2002.
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NYC-WTC_000037820
Log sheet recording sample preparation details including drip rates and pH for GCMS analysis in March 2002.
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NYC-WTC_000037825
Laboratory report listing quantitative concentrations of volatile organic compounds in sample AE00364 analyzed on March 21, 2002.
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NYC-WTC_000037829
Reference data report for GCMS analysis of sample AE00364 showing peak identification and response values from March 21, 2002.
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NYC-WTC_000037848
Laboratory report documenting GCMS analysis of a method blank for sample AE03799 to verify analytical system cleanliness.
Filed in the same folder