GCMS analysis results for sample AD31662, Feb 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\FEB1302\31662.D Vial: 6 Acq On : 13 Feb 2002 8:05 pm Operator: 209 GALOS Sample : GC/MS SCAN 2/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 15 9:58 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.34 152 311080 20.00 ug/1 0.00 10) Naphthalene-d8 15.99 136 1187663 20.00 ug/1 0.00 17) Acenaphthene-diO 21.30 164 636720 20.00 ug/1 0.00 29) Phenanthrene-diO 25.76 188 939869 20.00 ug/1 0.00 38) Chrysene-dl2 33.83 240 664630 20.00 ug/1 -0.02 44) Perylene-dl2 38.11 264 428648 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 30.83 235. 41714 4.42 ug/mL 0.34 Spiked Amount 5.000 Recovery = 88.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 12.24 146 185 N.D. 5) 1,4-Dichlorobenzene 12.38 146 282 N.D. 6) 1,2-Dichlorobenzene 12.91 146 189 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 14.69 82 125 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 16.03 128 1271 N.D. 16) Hexachlorobutadiene 16.59 225 562 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 19.56 162 199 N.D. 20) Dimethylphthalate 20.64 163 307 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 20.84 152 345 N.D. 2 3) Acenaphthene 21.40 153 378 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.77 149 396 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 31662.D GCMS0208.M Fri Feb 15 09:59:21 2002 Page 1

NYC-WTC_000005765