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GCMS blank analysis results for sample AE03508, March 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS blank analysis results for volatile organic compounds with detection limits below MDL.

NYC-WTC_000037616–000037634

Folder label: “GCMS X 2/19/02 A 3/8/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02MAR08\0219B.D Vial: 1 Acq On : 8 Mar 2002 10:39 am Operator: Sample : lab blank 2/19 Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 Butanoic acid, 2-methyl-, m. . Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 4.64 0.11 ug/L 52118 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Butanoic acid, 2-methyl-, methyl... 116 C6H12O2 000868-57-5 78 2 Butanoic acid, 2-methyl-, methyl... 116 C6H12O2 000868-57-5 64 3 Butanoic acid, 2-methyl-, methyl... 116 C6H12O2 000868-57-5 64 4 Butanoic acid, 2-methyl-, methyl... 116 C6H12O2 000868-57-5 56 Abundance Scan 112 (4.638 min): 0219B.D (-) m/z 88.00 100.00% 57 88

5000 43 101 71 - 111111_—IIEEOIII141115T 4.20 4.40 4.60 4.80 5.00 207 0 T’IUIITTTTTTUIITT mpM TTIM"Bp—agn, TUpTungur TIr Tur m/z 57.00 84.29% mz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190200210 Abundance #16440: Butanoic acid, 2-methyl-, methyl ester (CAS) $$ Me... 57 88

5000 - 11, ,,,, 101 4.20 4.40 4.60 4.80 5.00 ' 74 m/z 85.00 35.98%

tJz~> 0 151..... 1= 27 ..... I ‘I■■ i ■ 11—71411 TOTDtnuup,116 Ifi THggonv ,;« > . . ; . , , , ( , J .. I ■,. .pTTTp-n- 10 20 30 40 50 60 70 80 90 100 110 120130 140 150 160 170 180 190200210 Abundance #16434: Butanoic acid, 2-methyl-, methyl ester $$ Butyric... 57 88

4.20 4.40 4.60 4.80 5.00 5000 m/z 43.00 30.32% 27 101

miz-> r 69 0-■ ■ i ■ “ • i ■" ■ I ■ ■ ■ ■ i ■ “ ■ i" TTIOpTTT 10 20 30 40 50 60 70 80 90 100 110 120130 140150 160 170 180 190200210 Abundance #16441: Butanoic acid, 2-methyl-, methyl ester (CAS) $$ Me... 88 AAAAAMAA —AA 4.20 4.40 4.60 4.80 5.00 57 m/z 59.00 29.08% 5000 41 29 101 69 miz-> 0 1′111111111, r | I"'11 ■ T’Tf TT ».ft.।। m-rpTT rmp-rrrpn> q i in । > 1111 n i >| in 10 2030405060 70 8090 100 110120 130 140 150 160 170 180190200210 — .... AA 4.40 4.60 4.80 4.20

0219B.D HP022102.M Fri Mar 15 10:08:43 2002 Page 5

NYC-WTC_000037623

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NYC-WTC_000037623Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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