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GCMS blank analysis results for sample AE03508, March 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS blank analysis results for volatile organic compounds with detection limits below MDL.

NYC-WTC_000037616–000037634

Folder label: “GCMS X 2/19/02 A 3/8/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

* Data File : C:\MSDCHEM\l\5973N\02MAR08\0219B.D Vial: 1 Acq On : 8 Mar 2002 10:39 am Operator: Sample : lab blank 2/19 Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 Propane, 1,l-dimethoxy-2-me... Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

3.93 0.08 ug/L 39532 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Propane, 1,l-dimethoxy-2-methyl - 118 C6H1402 041632-89-7 78 2 ISOBUTYRALDEHYDE, DIMETHYLACETAL. .. 118 C6H14O2 000000-00-0 78 3 3-(Methylthio)-2-butanone $$ 2-B... 118 C5H10OS 053475-15-3 42 4 Heptane, 1,1-dimethoxy- (CAS) $$... 160 C9H20O2 010032-05-0 40 Abundance Scan 49 (3.927 min): 0219B.D (-) m/z 75.00 100.00% 75

5000 87 55 41 TP ■ ■ । ■ ■ ■ ■ i ■ ■ ■1 । ■ ' '' । 3.60 3.80 4,00 4.20 11 1l(.... ।.. . 1.! 1———— .. TII—00011100 207 m/z i87.10 47.37% 0- ।.।..... m/z—> 20 30 40 50 60 70 80 90 100110 120130140150160 170180 190200 21C Abundance #17846: Propane, 1,1-dimethoxy-2-methyl- 75

5000 87 ---------------- 3.60 3.80 4.00 4.20 -A— 55 m/z 55.00 30.24% 0 TTTppr -rrpT31 45i -HgDTmTT I TTIUOIUnpg] m/z—> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #17849: ISOBUTYRALDEHYDE, DIMETHYLACETAL $$ 1,1 -Dimethoxyi.. 75 —. —AA— 3.60 3.80 4.00 4.20 5000 m/z 47.00 16.70% 87 55 29 45 ... 0 1’11 »h। i < i . |lift 1 ili i j t . J l| 1127 | r t l. | . > | .... p > . . [ I M 1 | .... | ... .j .... | .... | ... .j .... | | .... ( . . , m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #17584: 3-(Methylthio)-2-butanone $$ 2-Butanone, 3-(methyl... ■ ' I ■ ■ • ‘ i T T 75 3.60 3.80 4.00 4.20 m/z 41.10 12.38% 5000 118 47

m/z—> 0- 59 mmmmmlmmmmp TuOuUngO]—np—B83,—mBIp—mBpp TIUT 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 _AAA 3.60 3.80 4.00 4.20

0219B.D HP022102.M Fri Mar 15 10:08:43 2002 Page 4

NYC-WTC_000037622

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NYC-WTC_000037622Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.995

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