GCMS reference standard results for volatile organics, Mar 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\MSDCHEM\l\5973N\02MAR08\0219Rl .D Vial: 2 Acq On : 8 Mar 2002 11:28 am Operator: Sample : ref 1 2/19 Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Mar 15 10:05:03 2002 Quant Results File: HP022102.RES Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Last Update : Mon Feb 25 10:47:59 2002 Response via : Initial Calibration DataAcq Meth : HP022102 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.71 152 1764249 20.00 ug/L 0.00 10) Naphthalene-d8 13.20 136 7753603 20.00 ug/L 0.00 17) Acenaphthene-diO 18.34 164 3989247 20.00 ug/L 0.00 29) Phenanthrene-diO 22.63 188 6701621 20.00 ug/L -0.01 38) Chrysene-dl2 30.49 240 5419486 20.00 ug/L -0.03 44) Perylene-dl2 34.41 264 3626472 20.00 ug/L -0.04 System Monitoring Compounds 37) 2,4-DDD 27.72 235 413436 4.63 ug/L 0.00 Spiked Amount 5.000 Recovery = 92.60% Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.99 74 419021 4.84 ug/L 100 3) bis(2-Chloroethyl)ether 9.24 93 1056094 9.16 ug/L 98 4) 1,3-Dichlorobenzene 9.61 146 747698 5.70 ug/L 99 5) 1,4-Dichlorobenzene 9.75 146 789461 6.05 ug/L 98 6) 1,2-Dichlorobenzene 10.24 146 789237 6.78 ug/L 96 7) 2,2'-oxybi s (1-Chioropropa 10.67 45 1569280 8.57 ug/L 96 8) n-Nitroso-di-n-propylamine 11.05 70 686747 7.98 ug/L 98 9) Hexachloroethane 11.03 117 201952 4.48 ug/L 96 11) Nitrobenzene 11.36 77 815937 5.99 ug/L 98 12) 1sophorone 12.02 82 2057772 7.86 ug/L 99 13) bis(2-Chloroethoxy)methane 12.77: 93 1266726 7.41 ug/L 98 14) 1,2,4-Trichlorobenzene 13.12 180 625736 6.24 ug/L 96 15) Naphthalene 13.24 128 2883283 7.52 ug/L 99 16) Hexachiorobutadiene 13.84 225 223743 4.57 ug/L 98 18) Hexachlorocyclopentadiene 15.95 237 53157 1.69 ug/L 95 19) 2-Chloronaphthalene 16.65 162 1626569 7.63 ug/L 96 20) Dimethylphthalate 17.89 163 2058142 8.50 ug/L 95 21) 2,6-Dinitrotoluene 18.06 165 262992 4.71 ug/L 99 22) Acenaphthylene 17.87 152 2605446 7.98 ug/L 99 2 3) Acenaphthene 18.42 153 1785851 8.30 ug/L 98 24) 2,4-Dinitrotoluene 19.18 165 320710 4.16 ug/L 99 25) Diethylphthalate 19.99 149 2126507 9.44 ug/L 99 26) 4-Chlorophenyl-phenylether 20.02 204 953916 9.36 ug/L 91 2 7) Fluorene 19.91 166 2108992 8.12 ug/L 100 28) Azobenzene/1,2-Diphenylhyd 20.47 77 2486690 8.37 ug/L 96 30) N-nitrosodiphenylamine 20.43 169 1253215 7.31 ug/L 98 31) 4-Bromophenyl-phenylether 21.44 248 525814 7.77 ug/L 97 3 2) Hexachlorobenzene 21.76 284 544724 7.73 ug/L 97 3 3) Phenanthrene 22.70 178 3240697 8.66 ug/L 99 3 4) Anthracene 22.82 178 3087335 8.19 ug/L 99 (#) = qualifier out of range (m) = manual integration 0219R1.D HP022102.M Tue Mar 19 11:13:17 2002 Page 1

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