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GCMS analysis results for sample AE03736, March 29, 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE03736 for unknown compounds conducted on March 29, 2002.

NYC-WTC_000037584–000037593

Folder label: “GCMS X 2/19/02 A 3/12/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

. Data File : C:\MSDCHEM\1\DATA\031202\3736.D Vial: 61 Acq On : 13 Mar 2002 7:08 am Operator: McLean Sample : SAMPLE 3736 2/19/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\5973N\5080302.M (RTF Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 10C Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 9.543 709 713 737 rBV 2598889 6727579 63.25% 11.757% 2 12.055 985 990 995 rVB 148008 256159 2.41% 0.448% 3 13.026 10'91 1097 1112 rBV 4769654 9378217 88.17% 16.390% 4 18.142 1654 1661 1675 rBV 4951427 10130594 95.24% 17.705% 5 22.495 2135 2141 2155 rBV2 4884168 10499215 98.71% 18.349%

6 27.430 2680 2685 2693 rBV 860965 1605073 15.09% 2.805% 7 30.314 2995 3003 3025 rBV2 4663726 10636527 100.00% 18.589% 8 30.613 3031 3036 3045 rBV 20G552 469439 4.41% 0.820% 9 30.913 3064 3069 3081 rBV 124075 303466 2.85% 0.530% 10 34.187 3422 3430 3449 rBV2 2898228 7213655 67.82% 12.607%

Sum of corrected areas: 57219924

3736.D 5080302.M Fri Mar 15 14:27:20 2002 Page 1

NYC-WTC_000037589

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NYC-WTC_000037589Source: NYC Law Department, mirrored locally

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